3,5-bis-O-(2,4-dichlorophenylmethyl)-2,4-di-C-methyl-1-O-methyl-α-D-ribofuranose

Base Information

Chemical Name:3,5-bis-O-(2,4-dichlorophenylmethyl)-2,4-di-C-methyl-1-O-methyl-α-D-ribofuranose
CAS No.:443642-78-2
Molecular Formula:C₂₂H₂₄Cl₄O₅
Molecular Weight:510.242
Hs Code.:

Synonyms:3,5-bis-O-(2,4-dichlorophenylmethyl)-2,4-di-C-methyl-1-O-methyl-α-D-ribofuranose

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Chemical Property of 3,5-bis-O-(2,4-dichlorophenylmethyl)-2,4-di-C-methyl-1-O-methyl-α-D-ribofuranose

Chemical Property:

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Technology Process of 3,5-bis-O-(2,4-dichlorophenylmethyl)-2,4-di-C-methyl-1-O-methyl-α-D-ribofuranose

There total 5 articles about 3,5-bis-O-(2,4-dichlorophenylmethyl)-2,4-di-C-methyl-1-O-methyl-α-D-ribofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 443642-77-1
3,5-bis-O-(2,4-dichlorophenylmethyl)-1-O-methyl-4-C-methyl-α-D-ribofuranose

: 75-16-1
methylmagnesium bromide

: 443642-78-2
3,5-bis-O-(2,4-dichlorophenylmethyl)-2,4-di-C-methyl-1-O-methyl-α-D-ribofuranose

Guidance literature:: 3,5-bis-O-(2,4-dichlorophenylmethyl)-1-O-methyl-4-C-methyl-α-D-ribofuranose; With Dess-Martin periodane; In dichloromethane; at 20 ℃;

methylmagnesium bromide; In diethyl ether; at -30 - -15 ℃; for 5h;

Reference yield:

Na₂S₂O_3.5H₂O: Na₂S₂O_3.5H₂O

: 443642-77-1
3,5-bis-O-(2,4-dichlorophenylmethyl)-1-O-methyl-4-C-methyl-α-D-ribofuranose

: 87413-09-0
Dess-Martin periodane

: 443642-78-2
3,5-bis-O-(2,4-dichlorophenylmethyl)-2,4-di-C-methyl-1-O-methyl-α-D-ribofuranose

Guidance literature:: With MeMgBr; In diethyl ether; dichloromethane; sodium hydrogencarbonate;

Reference yield:

: 582313-29-9
5-deoxy-1,2-O-isopropylidene-D-xylofuranose

: 443642-78-2
3,5-bis-O-(2,4-dichlorophenylmethyl)-2,4-di-C-methyl-1-O-methyl-α-D-ribofuranose

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; hydrogenchloride; potassium hydroxide; formaldehyd; NaH; acetic anhydride / 1,4-dioxane; 1-methyl-pyrrolidin-2-one; methanol; dichloromethane

2: MeMgBr / diethyl ether; dichloromethane; sodium hydrogencarbonate

With pyridine; hydrogenchloride; potassium hydroxide; formaldehyd; NaH; MeMgBr; acetic anhydride; In 1,4-dioxane; 1-methyl-pyrrolidin-2-one; methanol; diethyl ether; dichloromethane; sodium hydrogencarbonate;