di(tert-butyl) N-<3-<<(E)-3-(4-methoxyphenyl)prop-2-enoyl>amino>propyl>-N,N'-<(1,4-13C2)butane-1,4-diyl>bis

Base Information

Chemical Name:di(tert-butyl) N-<3-<<(E)-3-(4-methoxyphenyl)prop-2-enoyl>amino>propyl>-N,N'-<(1,4-13C2)butane-1,4-diyl>bis
CAS No.:219985-83-8
Molecular Formula:C₂₇H₄₃N₃O₆
Molecular Weight:507.633
Hs Code.:

di(tert-butyl) N-<3-<<(E)-3-(4-methoxyphenyl)prop-2-enoyl>amino>propyl>-N,N'-<(1,4-13C2)butane-1,4-diyl>bis<carbamate>

Synonyms:di(tert-butyl) N-<3-<<(E)-3-(4-methoxyphenyl)prop-2-enoyl>amino>propyl>-N,N'-<(1,4-13C2)butane-1,4-diyl>bis

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of di(tert-butyl) N-<3-<<(E)-3-(4-methoxyphenyl)prop-2-enoyl>amino>propyl>-N,N'-<(1,4-13C2)butane-1,4-diyl>bis

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Technology Process of di(tert-butyl) N-<3-<<(E)-3-(4-methoxyphenyl)prop-2-enoyl>amino>propyl>-N,N'-<(1,4-13C2)butane-1,4-diyl>bis

There total 7 articles about di(tert-butyl) N-<3-<<(E)-3-(4-methoxyphenyl)prop-2-enoyl>amino>propyl>-N,N'-<(1,4-13C2)butane-1,4-diyl>bis which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 34446-64-5,42996-84-9
(E)-3-(4-methoxyphenyl)propenoyl chloride

: 219985-82-7
di(tert-butyl) N-(3-aminopropyl)-N,N'-<(1,4-13C2)butane-1,4-diyl>bis

: 219985-83-8
di(tert-butyl) N-<3-<<(E)-3-(4-methoxyphenyl)prop-2-enoyl>amino>propyl>-N,N'-<(1,4-13C2)butane-1,4-diyl>bis

Guidance literature:: With triethylamine; In ethyl acetate; at 25 ℃;
DOI:10.1016/S0040-4020(98)01014-X

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 219985-83-8
di(tert-butyl) N-<3-<<(E)-3-(4-methoxyphenyl)prop-2-enoyl>amino>propyl>-N,N'-<(1,4-13C2)butane-1,4-diyl>bis

Guidance literature:: Multi-step reaction with 3 steps

1: 0.18 g / CH₂Cl₂ / 3 h / 25 °C

2: NaOH, Raney-Ni, H₂ / ethanol; H₂O / 20 h / 25 °C / 2068.59 Torr

3: 82 percent / Et₃N / ethyl acetate / 25 °C

With sodium hydroxide; hydrogen; nickel; triethylamine; In ethanol; dichloromethane; water; ethyl acetate;
DOI:10.1016/S0040-4020(98)01014-X

Reference yield:

: 943-89-5
(E)-3-(4-methoxyphenyl)acrylic acid

: 219985-83-8
di(tert-butyl) N-<3-<<(E)-3-(4-methoxyphenyl)prop-2-enoyl>amino>propyl>-N,N'-<(1,4-13C2)butane-1,4-diyl>bis

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / oxalyl chloride / toluene

2: 82 percent / Et₃N / ethyl acetate / 25 °C

With oxalyl dichloride; triethylamine; In ethyl acetate; toluene;
DOI:10.1016/S0040-4020(98)01014-X