1-(4,6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hexopyranosyl)-2-phenylethane

Base Information

Chemical Name:1-(4,6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hexopyranosyl)-2-phenylethane
CAS No.:1513884-72-4
Molecular Formula:C₁₈H₂₄O₅
Molecular Weight:320.386
Hs Code.:

Synonyms:1-(4,6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hexopyranosyl)-2-phenylethane

Suppliers and Price of 1-(4,6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hexopyranosyl)-2-phenylethane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(4,6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hexopyranosyl)-2-phenylethane

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Technology Process of 1-(4,6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hexopyranosyl)-2-phenylethane

There total 2 articles about 1-(4,6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hexopyranosyl)-2-phenylethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: (E)-1-(4,6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hex-2-enopyranosyl)-2-chloro-2-phenylethene

: 1513884-72-4
1-(4,6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hexopyranosyl)-2-phenylethane

Guidance literature:: With palladium 10% on activated carbon; hydrogen; triethylamine; for 10h;
DOI:10.1080/07328303.2013.860160

Reference yield:

: 536-74-3
phenylacetylene

: 2873-29-2
D-glucal triacetate

: 1513884-72-4
1-(4,6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hexopyranosyl)-2-phenylethane

Guidance literature:: Multi-step reaction with 2 steps

1: tin(IV) chloride / dichloromethane / 0.17 h / -45 °C

2: palladium 10% on activated carbon; hydrogen; triethylamine / 10 h

With palladium 10% on activated carbon; hydrogen; tin(IV) chloride; triethylamine; In dichloromethane; 1: |Ferrier Carbohydrate Rearrangement;
DOI:10.1080/07328303.2013.860160