Thiobrenzschleimsaeure-o-chloranilid

Base Information

• Chemical Name: Thiobrenzschleimsaeure-o-chloranilid
• CAS No.: 95322-68-2
• Molecular Formula: C₁₁H₈ClNOS
• Molecular Weight: 237.71
• Mol file: 95322-68-2.mol

Synonyms:Thiobrenzschleimsaeure-o-chloranilid

Chemical Property of Thiobrenzschleimsaeure-o-chloranilid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of Thiobrenzschleimsaeure-o-chloranilid

There total 4 articles about Thiobrenzschleimsaeure-o-chloranilid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(2-chlorophenyl)furan-2-carboxamide (58050-52-5) → Thiobrenzschleimsaeure-o-chloranilid (95322-68-2)

Guidance literature:

With tetraphosphorus decasulfide; In pyridine;

DOI:10.1016/S0957-4166(03)00025-9

Reference yield:

o-chloroaniline (95-51-2) → Thiobrenzschleimsaeure-o-chloranilid (95322-68-2)

Guidance literature:

Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 16 h / 0 - 25 °C

2: Lawessons reagent / toluene / 16 h / 110 °C

With Lawessons reagent; N-ethyl-N,N-diisopropylamine; In dichloromethane; toluene;

Reference yield:

2-furancarbonyl chloride (527-69-5) → Thiobrenzschleimsaeure-o-chloranilid (95322-68-2)

Guidance literature:

Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 16 h / 0 - 25 °C

2: Lawessons reagent / toluene / 16 h / 110 °C

With Lawessons reagent; N-ethyl-N,N-diisopropylamine; In dichloromethane; toluene;

upstream raw materials:

N-(2-chlorophenyl)furan-2-carboxamide

o-chloroaniline

2-furancarbonyl chloride