trifluoro-acetic acid, 1,4-butanediyl ester

Base Information

• Chemical Name: trifluoro-acetic acid, 1,4-butanediyl ester
• CAS No.: 31528-89-9
• Molecular Formula: C₈H₈F₆O₄
• Molecular Weight: 282.14

Synonyms:trifluoro-acetic acid, 1,4-butanediyl ester

Chemical Property of trifluoro-acetic acid, 1,4-butanediyl ester

Chemical Property:

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Technology Process of trifluoro-acetic acid, 1,4-butanediyl ester

There total 1 articles about trifluoro-acetic acid, 1,4-butanediyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

propane (74-98-6) + C10F11IO2 → isopropyl Trifluoroacetate (400-38-4) + trifluoro-acetic acid, 1,4-butanediyl ester (31528-89-9) + 1,2,3,4,5-pentafluoro-6-iodobenzene (827-15-6)

Guidance literature:

With trifluoroacetic acid; trifluoroacetic anhydride; at 150 ℃; Inert atmosphere;

DOI:10.1002/anie.201406185

Reference yield:

trifluoro-acetic acid, 1,4-butanediyl ester (31528-89-9) → 1,4-dibromo-butane (110-52-1)

Guidance literature:

With lithium bromide; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; for 4h; Yield given; Heating;

DOI:10.1055/s-1987-27988

upstream raw materials:

propane

Downstream raw materials:

1,4-dibromo-butane

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