benzyl (2-O-glycolyl-5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-β-O-manno-2-nonulopyranosid)onate

Base Information

• Chemical Name: benzyl (2-O-glycolyl-5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-β-O-manno-2-nonulopyranosid)onate
• CAS No.: 195251-41-3
• Molecular Formula: C₂₈H₃₇NO₁₄
• Molecular Weight: 611.6

Synonyms:benzyl (2-O-glycolyl-5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-β-O-manno-2-nonulopyranosid)onate

Chemical Property of benzyl (2-O-glycolyl-5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-β-O-manno-2-nonulopyranosid)onate

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Technology Process of benzyl (2-O-glycolyl-5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-β-O-manno-2-nonulopyranosid)onate

There total 1 articles about benzyl (2-O-glycolyl-5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-β-O-manno-2-nonulopyranosid)onate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

benzyl (5-acetamido-4,7,8,9-tetra-O-acetyl-2-chloro-3,5-dideoxy-D-glycero-α-D-galacto-non-2-ulpyranosid)onate (113757-77-0) + ethylene glycol (107-21-1) → benzyl (2-O-glycolyl-5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-β-O-manno-2-nonulopyranosid)onate (195251-41-3)

Guidance literature:

With 2,6-di-tert-butyl-pyridine; silver trifluoromethanesulfonate; calcium carbonate; In acetonitrile; at -20 - 20 ℃;

DOI:10.1139/V06-031

Reference yield: 86.7%

triethylammonium 1,2-dihexadecyl-glycerol-3-H-phosphonate + benzyl (2-O-glycolyl-5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-β-O-manno-2-nonulopyranosid)onate (195251-41-3) → [benzyl (2-O-glycolyl-5-acetamido-4,7,8,9-O-tetraacetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosyl)]-1,2-dihexadecyl-glycero-3-H-phosphonate

Guidance literature:

With pyridine; pivaloyl chloride; at 0 ℃; for 0.166667h;

DOI:10.1139/V06-031

upstream raw materials:

benzyl (5-acetamido-4,7,8,9-tetra-O-acetyl-2-chloro-3,5-dideoxy-D-glycero-α-D-galacto-non-2-ulpyranosid)onate

ethylene glycol

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