bis{2-[(pentafluorophenyl)amino]phenyl} thioether

Base Information

Chemical Name:bis{2-[(pentafluorophenyl)amino]phenyl} thioether
CAS No.:1403585-69-2
Molecular Formula:C₂₄H₁₀F₁₀N₂S
Molecular Weight:548.407
Hs Code.:

Synonyms:bis{2-[(pentafluorophenyl)amino]phenyl} thioether

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Chemical Property of bis{2-[(pentafluorophenyl)amino]phenyl} thioether

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Technology Process of bis{2-[(pentafluorophenyl)amino]phenyl} thioether

There total 1 articles about bis{2-[(pentafluorophenyl)amino]phenyl} thioether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 392-56-3
Hexafluorobenzene

: 5873-51-8
2,2'-thiodianiline

: 1403585-69-2
bis{2-[(pentafluorophenyl)amino]phenyl} thioether

Guidance literature:: 2,2'-thiodianiline; With n-butyllithium; 1,1,1,3,3,3-hexamethyl-disilazane; In tetrahydrofuran; hexane; at -78 ℃; Inert atmosphere;

Hexafluorobenzene; In tetrahydrofuran; hexane; at -78 - 25 ℃; for 4h; Inert atmosphere;
DOI:10.1002/ejic.201200363

Reference yield: 63.0%

: germanium(II) chloride dioxane

: 1403585-69-2
bis{2-[(pentafluorophenyl)amino]phenyl} thioether

: 18400-61-8
lithium bis(trimethylsilyl)amide diethyl etherate

: 1403585-80-7
GeC₆F₅NC₆H₄SC₆H₄NC₆F₅

Guidance literature:: In tetrahydrofuran; soln. of LiN(SiMe3)2*Et2O in thf added to stirred soln. of S(o-C6H4NHC6F5)2 in thf at -78°C, warmed to room temp., stirred for 1 h, cooled to -78°C; mixt. stirred at room temp. overnight; volatiles removed in vac., recrystd. from toluene; elem. anal.;
DOI:10.1002/ejic.201200363

Reference yield:

: 1403585-69-2
bis{2-[(pentafluorophenyl)amino]phenyl} thioether

: 1403585-85-2
Br₂Ge(C₆F₅NC₆H₄SC₆H₄NC₆F₅)

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran

2: toluene

In tetrahydrofuran; toluene;
DOI:10.1002/ejic.201200363