3-{3-(2-Ethoxycarbonyl-ethyl)-4-[(E)-6-(4-methanesulfonyl-phenyl)-hex-5-enyloxy]-benzoyl}-benzoic acid ethyl ester

Base Information

Chemical Name:3-{3-(2-Ethoxycarbonyl-ethyl)-4-[(E)-6-(4-methanesulfonyl-phenyl)-hex-5-enyloxy]-benzoyl}-benzoic acid ethyl ester
CAS No.:128577-83-3
Molecular Formula:C₃₄H₃₈O₈S
Molecular Weight:606.737
Hs Code.:

Synonyms:3-{3-(2-Ethoxycarbonyl-ethyl)-4-[(E)-6-(4-methanesulfonyl-phenyl)-hex-5-enyloxy]-benzoyl}-benzoic acid ethyl ester

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Chemical Property of 3-{3-(2-Ethoxycarbonyl-ethyl)-4-[(E)-6-(4-methanesulfonyl-phenyl)-hex-5-enyloxy]-benzoyl}-benzoic acid ethyl ester

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Technology Process of 3-{3-(2-Ethoxycarbonyl-ethyl)-4-[(E)-6-(4-methanesulfonyl-phenyl)-hex-5-enyloxy]-benzoyl}-benzoic acid ethyl ester

There total 11 articles about 3-{3-(2-Ethoxycarbonyl-ethyl)-4-[(E)-6-(4-methanesulfonyl-phenyl)-hex-5-enyloxy]-benzoyl}-benzoic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 128577-81-1
3-{3-(2-Ethoxycarbonyl-ethyl)-4-[(E)-6-(4-methylsulfanyl-phenyl)-hex-5-enyloxy]-benzoyl}-benzoic acid ethyl ester

: 128577-83-3
3-{3-(2-Ethoxycarbonyl-ethyl)-4-[(E)-6-(4-methanesulfonyl-phenyl)-hex-5-enyloxy]-benzoyl}-benzoic acid ethyl ester

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 25 ℃; for 2h;
DOI:10.1021/jm00172a020

Reference yield:

: 67326-20-9
3-carbethoxybenzoyl chloride

: 128577-83-3
3-{3-(2-Ethoxycarbonyl-ethyl)-4-[(E)-6-(4-methanesulfonyl-phenyl)-hex-5-enyloxy]-benzoyl}-benzoic acid ethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) AlCl₃ / 1.) CH₂Cl₂, 0 deg C, 1 h, 2.) 0 deg C, 4 h

2: 92 percent / pyridine hydrochloride / 4 h / 180 °C

3: 56 percent / sulfuric acid / 96 h / Heating

4: 1.) 60percent sodium hydride disp. in oil / 1.) DMF, 25 deg C, 30 min, 2.) 65 deg C

5: 68 percent / m-chloroperbenzoic acid (mCPBA) / CH₂Cl₂ / 2 h / 25 °C

With aluminium trichloride; sulfuric acid; pyridine hydrochloride; sodium hydride; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1021/jm00172a020

Reference yield:

: 70311-27-2
2-methoxybenzenepropanoic acid ethyl ester

: 128577-83-3
3-{3-(2-Ethoxycarbonyl-ethyl)-4-[(E)-6-(4-methanesulfonyl-phenyl)-hex-5-enyloxy]-benzoyl}-benzoic acid ethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) AlCl₃ / 1.) CH₂Cl₂, 0 deg C, 1 h, 2.) 0 deg C, 4 h

2: 92 percent / pyridine hydrochloride / 4 h / 180 °C

3: 56 percent / sulfuric acid / 96 h / Heating

4: 1.) 60percent sodium hydride disp. in oil / 1.) DMF, 25 deg C, 30 min, 2.) 65 deg C

5: 68 percent / m-chloroperbenzoic acid (mCPBA) / CH₂Cl₂ / 2 h / 25 °C

With aluminium trichloride; sulfuric acid; pyridine hydrochloride; sodium hydride; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1021/jm00172a020