Technology Process of C70H83NO17
There total 20 articles about C70H83NO17 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C54H63NO15;
With
di(n-butyl)tin oxide;
In
methanol;
for 2h;
Reflux;
benzyl (R)-3-cyclohexyl-2-(trifluorormethylsulfonyloxy)propanoate;
With
cesium fluoride;
In
1,2-dimethoxyethane;
at 20 ℃;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0.5 h / 20 °C
2.1: dichloromethane / 0.5 h / 20 °C / Molecular sieve
2.2: 2 h / 0 °C
3.1: sodium methylate; methanol / 2 h
3.2: IR-120 (H(1+)) resin
4.1: triethylamine / acetonitrile / 1.33 h / 0 °C
5.1: di(n-butyl)tin oxide / methanol / 2 h / Reflux
5.2: 20 °C
With
methanol; sodium methylate; di(n-butyl)tin oxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine;
In
methanol; dichloromethane; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: dichloromethane / 0.5 h / 20 °C / Molecular sieve
1.2: 2 h / 0 °C
2.1: sodium methylate; methanol / 2 h
2.2: IR-120 (H(1+)) resin
3.1: triethylamine / acetonitrile / 1.33 h / 0 °C
4.1: di(n-butyl)tin oxide / methanol / 2 h / Reflux
4.2: 20 °C
With
methanol; sodium methylate; di(n-butyl)tin oxide; triethylamine;
In
methanol; dichloromethane; acetonitrile;