3,3'-(1,2,4-thiadiazole-3,5-diyl)bis(4-amino-7-methyl-8-phenylpyrazolo[5,1-c][1,2,4]triazine)

Base Information

Chemical Name:3,3'-(1,2,4-thiadiazole-3,5-diyl)bis(4-amino-7-methyl-8-phenylpyrazolo[5,1-c][1,2,4]triazine)
CAS No.:1548258-62-3
Molecular Formula:C₂₆H₂₀N₁₂S
Molecular Weight:532.591
Hs Code.:

Synonyms:3,3'-(1,2,4-thiadiazole-3,5-diyl)bis(4-amino-7-methyl-8-phenylpyrazolo[5,1-c][1,2,4]triazine)

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Chemical Property of 3,3'-(1,2,4-thiadiazole-3,5-diyl)bis(4-amino-7-methyl-8-phenylpyrazolo[5,1-c][1,2,4]triazine)

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Technology Process of 3,3'-(1,2,4-thiadiazole-3,5-diyl)bis(4-amino-7-methyl-8-phenylpyrazolo[5,1-c][1,2,4]triazine)

There total 3 articles about 3,3'-(1,2,4-thiadiazole-3,5-diyl)bis(4-amino-7-methyl-8-phenylpyrazolo[5,1-c][1,2,4]triazine) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 1269093-71-1
4-amino-7-methyl-8-phenylpyrazolo[5,1-c][1,2,4]triazine-3-carbothioamide

: 1548258-62-3
3,3'-(1,2,4-thiadiazole-3,5-diyl)bis(4-amino-7-methyl-8-phenylpyrazolo[5,1-c][1,2,4]triazine)

Guidance literature:: With triisopropylamine; dihydrogen peroxide; In water; N,N-dimethyl-formamide; at 20 ℃; for 4h;
DOI:10.1016/j.tetlet.2014.01.010

Reference yield:

: 60419-81-0
3-methyl-4-phenyl-1H-pyrazol-5-amine

: 1548258-62-3
3,3'-(1,2,4-thiadiazole-3,5-diyl)bis(4-amino-7-methyl-8-phenylpyrazolo[5,1-c][1,2,4]triazine)

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium nitrite; hydrogenchloride / water / 0 °C

1.2: 1 h / 20 °C

2.1: N,N-dimethyl-formamide / 0.33 h / Heating

3.1: dihydrogen peroxide; triisopropylamine / N,N-dimethyl-formamide; water / 4 h / 20 °C

With hydrogenchloride; triisopropylamine; dihydrogen peroxide; sodium nitrite; In water; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2014.01.010

Reference yield:

: 1548258-72-5
C₁₃H₁₂N₆S

: 1548258-62-3
3,3'-(1,2,4-thiadiazole-3,5-diyl)bis(4-amino-7-methyl-8-phenylpyrazolo[5,1-c][1,2,4]triazine)

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide / 0.33 h / Heating

2: dihydrogen peroxide; triisopropylamine / N,N-dimethyl-formamide; water / 4 h / 20 °C

With triisopropylamine; dihydrogen peroxide; In water; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2014.01.010