allyl (3,4-di-O-benzyl-2-O-levulinoyl-α-L-rhamnopyranosyl)-(1→4)-(benzyl 2,3-di-O-benzyl-β-D-galactopyranosyluronate)-(1→3)-4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranoside

Base Information

Chemical Name:allyl (3,4-di-O-benzyl-2-O-levulinoyl-α-L-rhamnopyranosyl)-(1→4)-(benzyl 2,3-di-O-benzyl-β-D-galactopyranosyluronate)-(1→3)-4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranoside
CAS No.:1603827-06-0
Molecular Formula:C₇₇H₈₂Cl₃NO₁₈
Molecular Weight:1415.85
Hs Code.:

allyl (3,4-di-O-benzyl-2-O-levulinoyl-α-L-rhamnopyranosyl)-(1→4)-(benzyl 2,3-di-O-benzyl-β-D-galactopyranosyluronate)-(1→3)-4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranoside

Synonyms:allyl (3,4-di-O-benzyl-2-O-levulinoyl-α-L-rhamnopyranosyl)-(1→4)-(benzyl 2,3-di-O-benzyl-β-D-galactopyranosyluronate)-(1→3)-4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranoside

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Chemical Property of allyl (3,4-di-O-benzyl-2-O-levulinoyl-α-L-rhamnopyranosyl)-(1→4)-(benzyl 2,3-di-O-benzyl-β-D-galactopyranosyluronate)-(1→3)-4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranoside

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Technology Process of allyl (3,4-di-O-benzyl-2-O-levulinoyl-α-L-rhamnopyranosyl)-(1→4)-(benzyl 2,3-di-O-benzyl-β-D-galactopyranosyluronate)-(1→3)-4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranoside

There total 1 articles about allyl (3,4-di-O-benzyl-2-O-levulinoyl-α-L-rhamnopyranosyl)-(1→4)-(benzyl 2,3-di-O-benzyl-β-D-galactopyranosyluronate)-(1→3)-4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 824939-37-9
3,4-di-O-benzyl-2-O-levulinoyl-α-L-rhamnopyranosyl trichloroacetimidate

: 1603826-97-6
allyl (benzyl 2,3-di-O-benzyl-β-D-gatactopyranosyturonate)-(1→3)-4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranoside

: 1603827-06-0
allyl (3,4-di-O-benzyl-2-O-levulinoyl-α-L-rhamnopyranosyl)-(1→4)-(benzyl 2,3-di-O-benzyl-β-D-galactopyranosyluronate)-(1→3)-4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranoside

Guidance literature:: 3,4-di-O-benzyl-2-O-levulinoyl-α-L-rhamnopyranosyl trichloroacetimidate; allyl (benzyl 2,3-di-O-benzyl-β-D-gatactopyranosyturonate)-(1→3)-4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranoside; In toluene; at 20 ℃; for 1h; Molecular sieve; Inert atmosphere;

With trimethylsilyl trifluoromethanesulfonate; In toluene; at -10 ℃; for 0.333333h;

Reference yield: 92.0%

: 1603827-06-0
allyl (3,4-di-O-benzyl-2-O-levulinoyl-α-L-rhamnopyranosyl)-(1→4)-(benzyl 2,3-di-O-benzyl-β-D-galactopyranosyluronate)-(1→3)-4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranoside

: 1603827-12-8
C₇₂H₇₆Cl₃NO₁₆

Guidance literature:: With pyridine; hydrazine hydrate; acetic acid; at 0 - 20 ℃; for 1h; Inert atmosphere;

Reference yield:

: 1603827-06-0
allyl (3,4-di-O-benzyl-2-O-levulinoyl-α-L-rhamnopyranosyl)-(1→4)-(benzyl 2,3-di-O-benzyl-β-D-galactopyranosyluronate)-(1→3)-4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranoside

: 1603827-07-1
C₇₄H₇₈Cl₃NO₁₈

: 1603827-08-2
C₇₄H₇₈Cl₃NO₁₈

Guidance literature:: allyl (3,4-di-O-benzyl-2-O-levulinoyl-α-L-rhamnopyranosyl)-(1→4)-(benzyl 2,3-di-O-benzyl-β-D-galactopyranosyluronate)-(1→3)-4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranoside; With (1,5-cyclooctadiene)[bis(methyldiphenylphosphine)]iridium(I) hexafluorophosphate; hydrogen; In tetrahydrofuran; at 20 ℃; for 2h; Inert atmosphere;

With water; iodine; In tetrahydrofuran; at 20 ℃; for 1.5h; Overall yield = 96 %; Overall yield = 2.84 g;