3,4-di-O-benzyl-2-O-levulinoyl-α-L-rhamnopyranosyl trichloroacetimidate

Base Information

Chemical Name:3,4-di-O-benzyl-2-O-levulinoyl-α-L-rhamnopyranosyl trichloroacetimidate
CAS No.:824939-37-9
Molecular Formula:C₂₇H₃₀Cl₃NO₇
Molecular Weight:586.897
Hs Code.:

Synonyms:3,4-di-O-benzyl-2-O-levulinoyl-α-L-rhamnopyranosyl trichloroacetimidate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,4-di-O-benzyl-2-O-levulinoyl-α-L-rhamnopyranosyl trichloroacetimidate

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Technology Process of 3,4-di-O-benzyl-2-O-levulinoyl-α-L-rhamnopyranosyl trichloroacetimidate

There total 1 articles about 3,4-di-O-benzyl-2-O-levulinoyl-α-L-rhamnopyranosyl trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 3,4-di-O-benzyl-2-O-levulinoyl-α/β-L-rhamnopyranose

: 545-06-2
trichloroacetonitrile

: 824939-37-9
3,4-di-O-benzyl-2-O-levulinoyl-α-L-rhamnopyranosyl trichloroacetimidate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In 1,2-dichloro-ethane; at -5 ℃; for 0.166667h; Inert atmosphere;
DOI:10.1002/ejoc.200800693

Reference yield: 94.0%

: 824939-37-9
3,4-di-O-benzyl-2-O-levulinoyl-α-L-rhamnopyranosyl trichloroacetimidate

: 311797-10-1
benzyl (allyl 2,3-di-O-benzyl-β-D-galactopyranoside)uronate

: 1448429-74-0
benzyl (3,4-di-O-benzyl-2-O-levulinoyl-α-L-rhamnopyranosyl)-(1→4)-(allyl 2,3-di-O-benzyl-β-D-galactopyranoside)uronate

Guidance literature:: 3,4-di-O-benzyl-2-O-levulinoyl-α-L-rhamnopyranosyl trichloroacetimidate; benzyl (allyl 2,3-di-O-benzyl-β-D-galactopyranoside)uronate; In toluene; at 20 ℃; for 1h; Microwave irradiation; Inert atmosphere;

With trimethylsilyl trifluoromethanesulfonate; In toluene; at -10 ℃; for 0.5h; Inert atmosphere;
DOI:10.1002/ejoc.201300180

Reference yield: 92.0%

: 824939-37-9
3,4-di-O-benzyl-2-O-levulinoyl-α-L-rhamnopyranosyl trichloroacetimidate

: 1349065-06-0
allyl (3,4-di-O-benzyl-α-L-rhamnopyranosyl)-(1→3)-[2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl-(1→4)]-2-O-levulinoyl-α-L-rhamnopyranoside

: 1349065-33-3
allyl (3,4-di-O-benzyl-2-O-levulinoyl-α-L-rhamnopyranosyl)-(1→2)-(3,4-di-O-benzyl-α-L-rhamnopyranosyl)-(1→3)-[2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl-(1→4)]-2-O-levulinoyl-α-L-rhamnopyranoside

Guidance literature:: 3,4-di-O-benzyl-2-O-levulinoyl-α-L-rhamnopyranosyl trichloroacetimidate; allyl (3,4-di-O-benzyl-α-L-rhamnopyranosyl)-(1→3)-[2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl-(1→4)]-2-O-levulinoyl-α-L-rhamnopyranoside; In diethyl ether; at -10 ℃; for 0.5h; Inert atmosphere; Molecular sieve;

trimethylsilyl trifluoromethanesulfonate; In diethyl ether; at -10 - 20 ℃; for 1h; Inert atmosphere; Molecular sieve;