2-(2-hydroxyethoxy)-3,10-dimethoxy-5,6,7,8,13,13a-hexahydroisoquinolino[2,1-b]isoquinolin-9-yl benzenesulfonate

Base Information

Chemical Name:2-(2-hydroxyethoxy)-3,10-dimethoxy-5,6,7,8,13,13a-hexahydroisoquinolino[2,1-b]isoquinolin-9-yl benzenesulfonate
CAS No.:1233354-06-7
Molecular Formula:C₂₇H₂₉NO₇S
Molecular Weight:511.596
Hs Code.:

Synonyms:2-(2-hydroxyethoxy)-3,10-dimethoxy-5,6,7,8,13,13a-hexahydroisoquinolino[2,1-b]isoquinolin-9-yl benzenesulfonate

Suppliers and Price of 2-(2-hydroxyethoxy)-3,10-dimethoxy-5,6,7,8,13,13a-hexahydroisoquinolino[2,1-b]isoquinolin-9-yl benzenesulfonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-(2-hydroxyethoxy)-3,10-dimethoxy-5,6,7,8,13,13a-hexahydroisoquinolino[2,1-b]isoquinolin-9-yl benzenesulfonate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-(2-hydroxyethoxy)-3,10-dimethoxy-5,6,7,8,13,13a-hexahydroisoquinolino[2,1-b]isoquinolin-9-yl benzenesulfonate

There total 2 articles about 2-(2-hydroxyethoxy)-3,10-dimethoxy-5,6,7,8,13,13a-hexahydroisoquinolino[2,1-b]isoquinolin-9-yl benzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1233353-81-5
2-hydroxy-3,10-dimethoxy-5,6,7,8,13,13a-hexahydroisoquinolino[2,1-b]isoquinolin-9-yl benzenesulfonate

: 540-51-2
2-bromoethanol

: 1233354-06-7
2-(2-hydroxyethoxy)-3,10-dimethoxy-5,6,7,8,13,13a-hexahydroisoquinolino[2,1-b]isoquinolin-9-yl benzenesulfonate

Guidance literature:: With caesium carbonate; N,N-dimethyl-formamide; at 80 ℃;

Reference yield:

: 1860-57-7
[2-(4-benzyloxy-3-methoxyphenyl)ethyl]amine hydrochloride

: 1233354-06-7
2-(2-hydroxyethoxy)-3,10-dimethoxy-5,6,7,8,13,13a-hexahydroisoquinolino[2,1-b]isoquinolin-9-yl benzenesulfonate

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / methanol / 5 h / Reflux

2.1: trichlorophosphate / toluene / 2 h / 120 °C

2.2: 5 - 20 °C

3.1: hydrogen; palladium on activated charcoal / methanol / 75 °C / 15201 Torr

4.1: caesium carbonate / N,N-dimethyl-formamide / 80 °C

With palladium on activated charcoal; hydrogen; caesium carbonate; triethylamine; trichlorophosphate; In methanol; N,N-dimethyl-formamide; toluene;