Technology Process of <3,6-dimethoxy-2-(phenylethynyl)phenyl>methanone
There total 3 articles about <3,6-dimethoxy-2-(phenylethynyl)phenyl>methanone which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
3 A molecular sieve; pyridinium chlorochromate;
In
dichloromethane;
for 6h;
Ambient temperature;
DOI:10.1016/S0040-4020(01)88016-9
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1) n-BuLi / 1) hexane, ether, -78 deg C, 30 min, 2) hexane, ether, -78 to 0 deg C, 2 h
2: 85 percent / pyridinium chlorochromate, 3A mol. sieves / CH2Cl2 / 6 h / Ambient temperature
With
n-butyllithium; 3 A molecular sieve; pyridinium chlorochromate;
In
dichloromethane;
DOI:10.1016/S0040-4020(01)88016-9
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1) n-BuLi / 1) hexane, ether, -78 deg C, 30 min, 2) hexane, ether, -78 to 0 deg C, 2 h
2: 85 percent / pyridinium chlorochromate, 3A mol. sieves / CH2Cl2 / 6 h / Ambient temperature
With
n-butyllithium; 3 A molecular sieve; pyridinium chlorochromate;
In
dichloromethane;
DOI:10.1016/S0040-4020(01)88016-9
