bis{4-[1-(2-methacryloyloxy)ethoxy]ethoxy-butyl}(methylenedi-4,1-phenylene) biscarbamate

Base Information

Chemical Name:bis{4-[1-(2-methacryloyloxy)ethoxy]ethoxy-butyl}(methylenedi-4,1-phenylene) biscarbamate
CAS No.:1268836-80-1
Molecular Formula:C₃₉H₅₄N₂O₁₂
Molecular Weight:742.864
Hs Code.:

Synonyms:bis{4-[1-(2-methacryloyloxy)ethoxy]ethoxy-butyl}(methylenedi-4,1-phenylene) biscarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis{4-[1-(2-methacryloyloxy)ethoxy]ethoxy-butyl}(methylenedi-4,1-phenylene) biscarbamate

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Technology Process of bis{4-[1-(2-methacryloyloxy)ethoxy]ethoxy-butyl}(methylenedi-4,1-phenylene) biscarbamate

There total 2 articles about bis{4-[1-(2-methacryloyloxy)ethoxy]ethoxy-butyl}(methylenedi-4,1-phenylene) biscarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 868-77-9,141668-69-1,25736-86-1,82601-55-6,25249-16-5
2-methyl-2-propenoic acid 2-hydroxyethyl ester

: 196109-16-7
bis[4-(vinyloxy)butyl] (methylenedi-4,1-phenylene)-biscarbamate

: 1268836-80-1
bis{4-[1-(2-methacryloyloxy)ethoxy]ethoxy-butyl}(methylenedi-4,1-phenylene) biscarbamate

Guidance literature:: With 4-tert-Butylcatechol; toluene-4-sulfonic acid; In tetrahydrofuran; at 30 ℃; for 8h;
DOI:10.1016/j.cclet.2010.10.028

Reference yield:

: 17832-28-9
4-(vinyloxy)butan-1-ol

: 1268836-80-1
bis{4-[1-(2-methacryloyloxy)ethoxy]ethoxy-butyl}(methylenedi-4,1-phenylene) biscarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 12 h / 50 °C / Inert atmosphere

2: 4-tert-Butylcatechol; toluene-4-sulfonic acid / tetrahydrofuran / 8 h / 30 °C

With 4-tert-Butylcatechol; toluene-4-sulfonic acid; In tetrahydrofuran;
DOI:10.1016/j.cclet.2010.10.028