C₄₆H₅₁ClN₄O₇

Base Information

Chemical Name:C₄₆H₅₁ClN₄O₇
CAS No.:1448822-25-0
Molecular Formula:C₄₆H₅₁ClN₄O₇
Molecular Weight:807.387
Hs Code.:

C<sub>46</sub>H<sub>51</sub>ClN<sub>4</sub>O<sub>7</sub>

Synonyms:C₄₆H₅₁ClN₄O₇

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Chemical Property of C₄₆H₅₁ClN₄O₇

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Technology Process of C₄₆H₅₁ClN₄O₇

There total 6 articles about C₄₆H₅₁ClN₄O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: C₃₇H₃₆ClN₂O₆⁽¹⁺⁾

: 57260-71-6
1-t-Butoxycarbonylpiperazine

: 1448822-25-0
C₄₆H₅₁ClN₄O₇

Guidance literature:: With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In N,N-dimethyl-formamide; Inert atmosphere;

Reference yield:

: 2513-23-7
2'-Carboxy-5-chloro-2,4-dihydroxybenzophenone

: 1448822-25-0
C₄₆H₅₁ClN₄O₇

Guidance literature:: Multi-step reaction with 5 steps

1: trifluoroacetic acid / 4 h / 100 °C / Sealed tube

2: triethylamine / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

3: palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / toluene / 20.5 h / 20 - 100 °C / Inert atmosphere; Schlenk technique

4: hydrogenchloride / water; acetic acid / 2 h / 100 °C

5: triethylamine; 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / Inert atmosphere

With hydrogenchloride; 1-hydroxy-7-aza-benzotriazole; palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; In water; acetic acid; N,N-dimethyl-formamide; toluene;

Reference yield:

: 1448822-18-1
C₃₃H₃₁ClF₃NO₈S

: 1448822-25-0
C₄₆H₅₁ClN₄O₇

Guidance literature:: Multi-step reaction with 3 steps

1: palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / toluene / 20.5 h / 20 - 100 °C / Inert atmosphere; Schlenk technique

2: hydrogenchloride / water; acetic acid / 2 h / 100 °C

3: triethylamine; 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / Inert atmosphere

With hydrogenchloride; 1-hydroxy-7-aza-benzotriazole; palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In water; acetic acid; N,N-dimethyl-formamide; toluene;