9-methoxycarbonyl-11-phenyl-4,9-dihydro-benzo[h]thieno [2,3-b]quinoline

Base Information

Chemical Name:9-methoxycarbonyl-11-phenyl-4,9-dihydro-benzo[h]thieno [2,3-b]quinoline
CAS No.:1379764-27-8
Molecular Formula:C₂₃H₁₇NO₂S
Molecular Weight:371.459
Hs Code.:

Synonyms:9-methoxycarbonyl-11-phenyl-4,9-dihydro-benzo[h]thieno [2,3-b]quinoline

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Chemical Property of 9-methoxycarbonyl-11-phenyl-4,9-dihydro-benzo[h]thieno [2,3-b]quinoline

Chemical Property:

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Technology Process of 9-methoxycarbonyl-11-phenyl-4,9-dihydro-benzo[h]thieno [2,3-b]quinoline

There total 4 articles about 9-methoxycarbonyl-11-phenyl-4,9-dihydro-benzo[h]thieno [2,3-b]quinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1379764-15-4
9-(methoxycarbonyl)-11-phenyl-benzo[h]thieno[2,3-b]quinolinium perchlorate

: 1379764-27-8
9-methoxycarbonyl-11-phenyl-4,9-dihydro-benzo[h]thieno [2,3-b]quinoline

Guidance literature:: With sodium tetrahydroborate; at 20 ℃;
DOI:10.3998/ark.5550190.0013.325

Reference yield:

: 1-chloro-3-dimethylamino-1-(N-(1-naphthyl)-N-phenyl)propeniminium perchlorate

: 1379764-27-8
9-methoxycarbonyl-11-phenyl-4,9-dihydro-benzo[h]thieno [2,3-b]quinoline

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium methylate / acetonitrile / 20 °C / pH > 9

2.1: trichlorophosphate / 0.33 h / 60 °C / Cooling

2.2: Cooling

3.1: sodium tetrahydroborate / 20 °C

With sodium tetrahydroborate; sodium methylate; trichlorophosphate; In acetonitrile;
DOI:10.3998/ark.5550190.0013.325

Reference yield:

: 59130-78-8
N-(1-naphthyl)-N-phenyl-acetamide

: 1379764-27-8
9-methoxycarbonyl-11-phenyl-4,9-dihydro-benzo[h]thieno [2,3-b]quinoline

Guidance literature:: Multi-step reaction with 4 steps

1.1: trichlorophosphate / 20 °C / Cooling

2.1: sodium methylate / acetonitrile / 20 °C / pH > 9

3.1: trichlorophosphate / 0.33 h / 60 °C / Cooling

3.2: Cooling

4.1: sodium tetrahydroborate / 20 °C

With sodium tetrahydroborate; sodium methylate; trichlorophosphate; In acetonitrile;
DOI:10.3998/ark.5550190.0013.325