9-(methoxycarbonyl)-11-phenyl-benzo[h]thieno[2,3-b]quinolinium perchlorate

Base Information

Chemical Name:9-(methoxycarbonyl)-11-phenyl-benzo[h]thieno[2,3-b]quinolinium perchlorate
CAS No.:1379764-15-4
Molecular Formula:C₂₃H₁₆NO₂S*ClO₄
Molecular Weight:469.902
Hs Code.:

Synonyms:9-(methoxycarbonyl)-11-phenyl-benzo[h]thieno[2,3-b]quinolinium perchlorate

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Chemical Property of 9-(methoxycarbonyl)-11-phenyl-benzo[h]thieno[2,3-b]quinolinium perchlorate

Chemical Property:

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Technology Process of 9-(methoxycarbonyl)-11-phenyl-benzo[h]thieno[2,3-b]quinolinium perchlorate

There total 3 articles about 9-(methoxycarbonyl)-11-phenyl-benzo[h]thieno[2,3-b]quinolinium perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 1065106-75-3
methyl 2-[(naphthalen-1-yl)(phenyl)amino]thiophene-5-carboxylate

: 1379764-15-4
9-(methoxycarbonyl)-11-phenyl-benzo[h]thieno[2,3-b]quinolinium perchlorate

Guidance literature:: N,N-dimethyl-formamide; methyl 2-[(naphthalen-1-yl)(phenyl)amino]thiophene-5-carboxylate; With trichlorophosphate; at 60 ℃; for 0.333333h; Cooling;

With perchloric acid; In methanol; Cooling;
DOI:10.3998/ark.5550190.0013.325

Reference yield:

: 1-chloro-3-dimethylamino-1-(N-(1-naphthyl)-N-phenyl)propeniminium perchlorate

: 1379764-15-4
9-(methoxycarbonyl)-11-phenyl-benzo[h]thieno[2,3-b]quinolinium perchlorate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium methylate / acetonitrile / 20 °C / pH > 9

2.1: trichlorophosphate / 0.33 h / 60 °C / Cooling

2.2: Cooling

With sodium methylate; trichlorophosphate; In acetonitrile;
DOI:10.3998/ark.5550190.0013.325

Reference yield:

: 59130-78-8
N-(1-naphthyl)-N-phenyl-acetamide

: 1379764-15-4
9-(methoxycarbonyl)-11-phenyl-benzo[h]thieno[2,3-b]quinolinium perchlorate

Guidance literature:: Multi-step reaction with 3 steps

1.1: trichlorophosphate / 20 °C / Cooling

2.1: sodium methylate / acetonitrile / 20 °C / pH > 9

3.1: trichlorophosphate / 0.33 h / 60 °C / Cooling

3.2: Cooling

With sodium methylate; trichlorophosphate; In acetonitrile;
DOI:10.3998/ark.5550190.0013.325