5-(3-Carboxybenzoyl)-2-{[6-(4-methyl-sulfinylphenyl)-5-hexenyl]oxy}benzenepropanoic acid

Base Information

Chemical Name:5-(3-Carboxybenzoyl)-2-{[6-(4-methyl-sulfinylphenyl)-5-hexenyl]oxy}benzenepropanoic acid
CAS No.:128599-34-8
Molecular Formula:C₃₀H₃₀O₇S
Molecular Weight:534.63
Hs Code.:

Synonyms:5-(3-Carboxybenzoyl)-2-{[6-(4-methyl-sulfinylphenyl)-5-hexenyl]oxy}benzenepropanoic acid

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Chemical Property of 5-(3-Carboxybenzoyl)-2-{[6-(4-methyl-sulfinylphenyl)-5-hexenyl]oxy}benzenepropanoic acid

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Technology Process of 5-(3-Carboxybenzoyl)-2-{[6-(4-methyl-sulfinylphenyl)-5-hexenyl]oxy}benzenepropanoic acid

There total 13 articles about 5-(3-Carboxybenzoyl)-2-{[6-(4-methyl-sulfinylphenyl)-5-hexenyl]oxy}benzenepropanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 128577-82-2
3-{3-(2-Ethoxycarbonyl-ethyl)-4-[(E)-6-(4-methanesulfinyl-phenyl)-hex-5-enyloxy]-benzoyl}-benzoic acid ethyl ester

: 128599-34-8
5-(3-Carboxybenzoyl)-2-{[6-(4-methyl-sulfinylphenyl)-5-hexenyl]oxy}benzenepropanoic acid

Guidance literature:: With potassium hydroxide; In ethanol; at 25 ℃; for 1h;
DOI:10.1021/jm00172a020

Reference yield:

: 67326-20-9
3-carbethoxybenzoyl chloride

: 128599-34-8
5-(3-Carboxybenzoyl)-2-{[6-(4-methyl-sulfinylphenyl)-5-hexenyl]oxy}benzenepropanoic acid

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) AlCl₃ / 1.) CH₂Cl₂, 0 deg C, 1 h, 2.) 0 deg C, 4 h

2: 92 percent / pyridine hydrochloride / 4 h / 180 °C

3: 56 percent / sulfuric acid / 96 h / Heating

4: 1.) 60percent sodium hydride disp. in oil / 1.) DMF, 25 deg C, 30 min, 2.) 65 deg C

5: 73 percent / m-chloroperbenzoic acid (mCPBA) / CH₂Cl₂ / 1.) -78 deg C, 5 min, 2.) warming up, 10 min

6: 56 percent / KOH / aq. ethanol / 1 h / 25 °C

With potassium hydroxide; aluminium trichloride; sulfuric acid; pyridine hydrochloride; sodium hydride; 3-chloro-benzenecarboperoxoic acid; In ethanol; dichloromethane;
DOI:10.1021/jm00172a020

Reference yield:

: 70311-27-2
2-methoxybenzenepropanoic acid ethyl ester

: 128599-34-8
5-(3-Carboxybenzoyl)-2-{[6-(4-methyl-sulfinylphenyl)-5-hexenyl]oxy}benzenepropanoic acid

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) AlCl₃ / 1.) CH₂Cl₂, 0 deg C, 1 h, 2.) 0 deg C, 4 h

2: 92 percent / pyridine hydrochloride / 4 h / 180 °C

3: 56 percent / sulfuric acid / 96 h / Heating

4: 1.) 60percent sodium hydride disp. in oil / 1.) DMF, 25 deg C, 30 min, 2.) 65 deg C

5: 73 percent / m-chloroperbenzoic acid (mCPBA) / CH₂Cl₂ / 1.) -78 deg C, 5 min, 2.) warming up, 10 min

6: 56 percent / KOH / aq. ethanol / 1 h / 25 °C

With potassium hydroxide; aluminium trichloride; sulfuric acid; pyridine hydrochloride; sodium hydride; 3-chloro-benzenecarboperoxoic acid; In ethanol; dichloromethane;
DOI:10.1021/jm00172a020