2-[7-(cyclohexylmethyl)-1,6-dihydro-2H-indeno[5,4-b]furan-8-yl]ethanamine hydrochloride

Base Information

Chemical Name:2-[7-(cyclohexylmethyl)-1,6-dihydro-2H-indeno[5,4-b]furan-8-yl]ethanamine hydrochloride
CAS No.:1287785-51-6
Molecular Formula:C₂₀H₂₇NO*ClH
Molecular Weight:333.901
Hs Code.:

Synonyms:2-[7-(cyclohexylmethyl)-1,6-dihydro-2H-indeno[5,4-b]furan-8-yl]ethanamine hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-[7-(cyclohexylmethyl)-1,6-dihydro-2H-indeno[5,4-b]furan-8-yl]ethanamine hydrochloride

Chemical Property:

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Technology Process of 2-[7-(cyclohexylmethyl)-1,6-dihydro-2H-indeno[5,4-b]furan-8-yl]ethanamine hydrochloride

There total 6 articles about 2-[7-(cyclohexylmethyl)-1,6-dihydro-2H-indeno[5,4-b]furan-8-yl]ethanamine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₀H₂₇NO

: 1287785-51-6
2-[7-(cyclohexylmethyl)-1,6-dihydro-2H-indeno[5,4-b]furan-8-yl]ethanamine hydrochloride

Guidance literature:: With hydrogenchloride; In methanol; ethyl acetate; at 60 ℃; for 3h;
DOI:10.1021/jm200221q

Reference yield:

: 1287785-42-5
7-(cyclohexylmethyl)-1,2,6,7-tetrahydro-8H-indeno[5,4-b]-furan-8-one

: 1287785-51-6
2-[7-(cyclohexylmethyl)-1,6-dihydro-2H-indeno[5,4-b]furan-8-yl]ethanamine hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 20 °C

1.2: 1 h / 40 °C

2.1: ammonia; hydrogen / ethanol / 72 h / 20 °C

3.1: hydrogenchloride / methanol; ethyl acetate / 3 h / 60 °C

With hydrogenchloride; ammonia; hydrogen; sodium hydride; In tetrahydrofuran; methanol; ethanol; ethyl acetate; mineral oil; 1.1: Horner-Wadsworth-Emmons olefination / 1.2: Horner-Wadsworth-Emmons olefination;
DOI:10.1021/jm200221q

Reference yield:

: C₂₀H₂₃NO

: 1287785-51-6
2-[7-(cyclohexylmethyl)-1,6-dihydro-2H-indeno[5,4-b]furan-8-yl]ethanamine hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: ammonia; hydrogen / ethanol / 72 h / 20 °C

2: hydrogenchloride / methanol; ethyl acetate / 3 h / 60 °C

With hydrogenchloride; ammonia; hydrogen; In methanol; ethanol; ethyl acetate;
DOI:10.1021/jm200221q