9-[4-(3,5-dimethyl-benzyl)-5-ethyl-6-methyl-2-oxo-1,2-dihydro-pyridin-3-ylcarbamoyl]-nonanoic acid

Base Information

Chemical Name:9-[4-(3,5-dimethyl-benzyl)-5-ethyl-6-methyl-2-oxo-1,2-dihydro-pyridin-3-ylcarbamoyl]-nonanoic acid
CAS No.:279220-42-7
Molecular Formula:C₂₇H₃₈N₂O₄
Molecular Weight:454.61
Hs Code.:

Synonyms:9-[4-(3,5-dimethyl-benzyl)-5-ethyl-6-methyl-2-oxo-1,2-dihydro-pyridin-3-ylcarbamoyl]-nonanoic acid

Suppliers and Price of 9-[4-(3,5-dimethyl-benzyl)-5-ethyl-6-methyl-2-oxo-1,2-dihydro-pyridin-3-ylcarbamoyl]-nonanoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 9-[4-(3,5-dimethyl-benzyl)-5-ethyl-6-methyl-2-oxo-1,2-dihydro-pyridin-3-ylcarbamoyl]-nonanoic acid

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 9-[4-(3,5-dimethyl-benzyl)-5-ethyl-6-methyl-2-oxo-1,2-dihydro-pyridin-3-ylcarbamoyl]-nonanoic acid

There total 3 articles about 9-[4-(3,5-dimethyl-benzyl)-5-ethyl-6-methyl-2-oxo-1,2-dihydro-pyridin-3-ylcarbamoyl]-nonanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 279220-38-1
9-[4-(3,5-dimethyl-benzyl)-5-ethyl-6-methyl-2-oxo-1,2-dihydro-pyridin-3-ylcarbamoyl]-nonanoic acid methyl ester

: 279220-42-7
9-[4-(3,5-dimethyl-benzyl)-5-ethyl-6-methyl-2-oxo-1,2-dihydro-pyridin-3-ylcarbamoyl]-nonanoic acid

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; methanol; at 20 ℃; for 0.0833333h;
DOI:10.1021/jm991125l

Reference yield:

: 818-88-2
sebacic acid mono methyl ester

: 279220-42-7
9-[4-(3,5-dimethyl-benzyl)-5-ethyl-6-methyl-2-oxo-1,2-dihydro-pyridin-3-ylcarbamoyl]-nonanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: hydroxybenzotriazole / CH₂Cl₂ / 0.58 h / 0 °C

2: hydroxybenzotriazole; N-methylmorpholine / CH₂Cl₂ / 19 h / 0 - 20 °C

3: 97 percent / aq. 4 N NaOH / tetrahydrofuran; methanol / 0.08 h / 20 °C

With 4-methyl-morpholine; sodium hydroxide; benzotriazol-1-ol; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jm991125l

Reference yield:

: 10-(N,N'-dicyclohexyl-carbamimidoyloxy)-10-oxo-decanoic acid methyl ester

: 279220-42-7
9-[4-(3,5-dimethyl-benzyl)-5-ethyl-6-methyl-2-oxo-1,2-dihydro-pyridin-3-ylcarbamoyl]-nonanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: hydroxybenzotriazole; N-methylmorpholine / CH₂Cl₂ / 19 h / 0 - 20 °C

2: 97 percent / aq. 4 N NaOH / tetrahydrofuran; methanol / 0.08 h / 20 °C

With 4-methyl-morpholine; sodium hydroxide; benzotriazol-1-ol; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jm991125l