9-[4-(3,5-dimethyl-benzyl)-5-ethyl-6-methyl-2-oxo-1,2-dihydro-pyridin-3-ylcarbamoyl]-nonanoic acid methyl ester

Base Information

• Chemical Name: 9-[4-(3,5-dimethyl-benzyl)-5-ethyl-6-methyl-2-oxo-1,2-dihydro-pyridin-3-ylcarbamoyl]-nonanoic acid methyl ester
• CAS No.: 279220-38-1
• Molecular Formula: C₂₈H₄₀N₂O₄
• Molecular Weight: 468.637

Synonyms:9-[4-(3,5-dimethyl-benzyl)-5-ethyl-6-methyl-2-oxo-1,2-dihydro-pyridin-3-ylcarbamoyl]-nonanoic acid methyl ester

Chemical Property of 9-[4-(3,5-dimethyl-benzyl)-5-ethyl-6-methyl-2-oxo-1,2-dihydro-pyridin-3-ylcarbamoyl]-nonanoic acid methyl ester

Chemical Property:

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Technology Process of 9-[4-(3,5-dimethyl-benzyl)-5-ethyl-6-methyl-2-oxo-1,2-dihydro-pyridin-3-ylcarbamoyl]-nonanoic acid methyl ester

There total 2 articles about 9-[4-(3,5-dimethyl-benzyl)-5-ethyl-6-methyl-2-oxo-1,2-dihydro-pyridin-3-ylcarbamoyl]-nonanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-amino-4-(3,5-dimethylbenzyl)-5-ethyl-6-methylpyridin-2(1H)-one (248246-95-9) + 10-(N,N'-dicyclohexyl-carbamimidoyloxy)-10-oxo-decanoic acid methyl ester → 9-[4-(3,5-dimethyl-benzyl)-5-ethyl-6-methyl-2-oxo-1,2-dihydro-pyridin-3-ylcarbamoyl]-nonanoic acid methyl ester (279220-38-1)

Guidance literature:

With 4-methyl-morpholine; benzotriazol-1-ol; In dichloromethane; at 0 - 20 ℃; for 19h;

DOI:10.1021/jm991125l

Reference yield:

sebacic acid mono methyl ester (818-88-2) → 9-[4-(3,5-dimethyl-benzyl)-5-ethyl-6-methyl-2-oxo-1,2-dihydro-pyridin-3-ylcarbamoyl]-nonanoic acid methyl ester (279220-38-1)

Guidance literature:

Multi-step reaction with 2 steps

1: hydroxybenzotriazole / CH₂Cl₂ / 0.58 h / 0 °C

2: hydroxybenzotriazole; N-methylmorpholine / CH₂Cl₂ / 19 h / 0 - 20 °C

With 4-methyl-morpholine; benzotriazol-1-ol; In dichloromethane;

DOI:10.1021/jm991125l

Reference yield: 97.0%

9-[4-(3,5-dimethyl-benzyl)-5-ethyl-6-methyl-2-oxo-1,2-dihydro-pyridin-3-ylcarbamoyl]-nonanoic acid methyl ester (279220-38-1) → 9-[4-(3,5-dimethyl-benzyl)-5-ethyl-6-methyl-2-oxo-1,2-dihydro-pyridin-3-ylcarbamoyl]-nonanoic acid (279220-42-7)

Guidance literature:

With sodium hydroxide; In tetrahydrofuran; methanol; at 20 ℃; for 0.0833333h;

DOI:10.1021/jm991125l

upstream raw materials:

3-amino-4-(3,5-dimethylbenzyl)-5-ethyl-6-methylpyridin-2(1H)-one

sebacic acid mono methyl ester

Downstream raw materials:

9-[4-(3,5-dimethyl-benzyl)-5-ethyl-6-methyl-2-oxo-1,2-dihydro-pyridin-3-ylcarbamoyl]-nonanoic acid

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