4-[[(2,6-Dichlorophenyl)carbonyl]amino]-N-[[1-(butyl)cyclopentyl]carbonyl]-L-phenylalanine Methyl Ester

Base Information

• Chemical Name: 4-[[(2,6-Dichlorophenyl)carbonyl]amino]-N-[[1-(butyl)cyclopentyl]carbonyl]-L-phenylalanine Methyl Ester
• CAS No.: 220878-44-4
• Molecular Formula: C₂₇H₃₂Cl₂N₂O₄
• Molecular Weight: 519.468

Synonyms:4-[[(2,6-Dichlorophenyl)carbonyl]amino]-N-[[1-(butyl)cyclopentyl]carbonyl]-L-phenylalanine Methyl Ester

Chemical Property of 4-[[(2,6-Dichlorophenyl)carbonyl]amino]-N-[[1-(butyl)cyclopentyl]carbonyl]-L-phenylalanine Methyl Ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of 4-[[(2,6-Dichlorophenyl)carbonyl]amino]-N-[[1-(butyl)cyclopentyl]carbonyl]-L-phenylalanine Methyl Ester

There total 4 articles about 4-[[(2,6-Dichlorophenyl)carbonyl]amino]-N-[[1-(butyl)cyclopentyl]carbonyl]-L-phenylalanine Methyl Ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-[[(2,6-dichlorophenyl)carbonyl]amino]-N-[[1-(3-butenyl)cyclopentyl]carbonyl]-L-phenylalanine methyl ester (220878-70-6) → 4-[[(2,6-Dichlorophenyl)carbonyl]amino]-N-[[1-(butyl)cyclopentyl]carbonyl]-L-phenylalanine Methyl Ester (220878-44-4)

Guidance literature:

palladium; In ethanol;

Reference yield:

1-Butyl-cyclopentanecarboxylic acid (62410-33-7) + 4-[[(2,6-dichlorophenyl)carbonyl]amino]-L-phenylalanine methyl ester hydrochloride → 4-[[(2,6-Dichlorophenyl)carbonyl]amino]-N-[[1-(butyl)cyclopentyl]carbonyl]-L-phenylalanine Methyl Ester (220878-44-4)

Guidance literature:

With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃;

DOI:10.1016/S0960-894X(02)00386-4

Reference yield:

methyl cyclopentane carboxylate (4630-80-2) → 4-[[(2,6-Dichlorophenyl)carbonyl]amino]-N-[[1-(butyl)cyclopentyl]carbonyl]-L-phenylalanine Methyl Ester (220878-44-4)

Guidance literature:

Multi-step reaction with 3 steps

1: LDA / tetrahydrofuran / 15 h / -70 - 20 °C

2: 1.0 N NaOH / methanol; tetrahydrofuran / 15 h / Heating

3: HBTU; DIPEA / dimethylformamide / 20 °C

With sodium hydroxide; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; lithium diisopropyl amide; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;

DOI:10.1016/S0960-894X(02)00386-4

upstream raw materials:

1-Butyl-cyclopentanecarboxylic acid

methyl cyclopentane carboxylate

1-Butyl-cyclopentanecarboxylic acid methyl ester

4-[[(2,6-dichlorophenyl)carbonyl]amino]-N-[[1-(3-butenyl)cyclopentyl]carbonyl]-L-phenylalanine methyl ester

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