2-[difluoro-(2,2,3,3,4,4,5,5-octafluoropyrrolidin-1-yl)methyl]-2,3,3,3-tetrafluoro-propanoyl fluoride

Base Information

• Chemical Name: 2-[difluoro-(2,2,3,3,4,4,5,5-octafluoropyrrolidin-1-yl)methyl]-2,3,3,3-tetrafluoro-propanoyl fluoride
• CAS No.: 122531-26-4
• Molecular Formula: C₈F₁₅NO
• Molecular Weight: 411.07
• Mol file: 122531-26-4.mol

Synonyms:2-[difluoro-(2,2,3,3,4,4,5,5-octafluoropyrrolidin-1-yl)methyl]-2,3,3,3-tetrafluoro-propanoyl fluoride

Chemical Property of 2-[difluoro-(2,2,3,3,4,4,5,5-octafluoropyrrolidin-1-yl)methyl]-2,3,3,3-tetrafluoro-propanoyl fluoride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-[difluoro-(2,2,3,3,4,4,5,5-octafluoropyrrolidin-1-yl)methyl]-2,3,3,3-tetrafluoro-propanoyl fluoride

There total 2 articles about 2-[difluoro-(2,2,3,3,4,4,5,5-octafluoropyrrolidin-1-yl)methyl]-2,3,3,3-tetrafluoro-propanoyl fluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.3%

2-methyl-3-pyrrolidin-1-yl-propionic acid methyl ester (4151-03-5) → perfluorobutane (355-25-9) + perfluoroisobutyryl fluoride (677-84-9) + 2-[difluoro-(2,2,3,3,4,4,5,5-octafluoropyrrolidin-1-yl)methyl]-2,3,3,3-tetrafluoro-propanoyl fluoride (122531-26-4) + perfluoro(N-propylpyrrolidine) (53708-07-9)

Guidance literature:

With hydrogen fluoride; at 7 - 8 ℃; for 8.08333h; Further byproducts given; electrochemical reaction; anodic current density of 3.5 A dm^-2, a cell voltage of 6.5 V - 6.7 V;

DOI:10.1016/0022-1139(93)03019-I

Reference yield: 43.3%

2-methyl-3-pyrrolidin-1-yl-propionic acid methyl ester (4151-03-5) → perfluorobutane (355-25-9) + 2-[difluoro-(2,2,3,3,4,4,5,5-octafluoropyrrolidin-1-yl)methyl]-2,3,3,3-tetrafluoro-propanoyl fluoride (122531-26-4) + 1-pentafluoroethyl-octafluoropyrrolidine (78159-15-6) + perfluoro(N-propylpyrrolidine) (53708-07-9)

Guidance literature:

With hydrogen fluoride; at 7 - 8 ℃; for 8.08333h; Further byproducts given; electrochemical reaction; anodic current density of 3.5 A dm^-2, a cell voltage of 6.5 V - 6.7 V;

DOI:10.1016/0022-1139(93)03019-I

upstream raw materials:

2-methyl-3-pyrrolidin-1-yl-propionic acid methyl ester