6-[4-(2-fluoroethoxy)phenyl]-5-methyl-5,6-dihydrophenanthridine-3,8-diamine

Base Information

Chemical Name:6-[4-(2-fluoroethoxy)phenyl]-5-methyl-5,6-dihydrophenanthridine-3,8-diamine
CAS No.:1314081-13-4
Molecular Formula:C₂₂H₂₂FN₃O
Molecular Weight:363.435
Hs Code.:

Synonyms:6-[4-(2-fluoroethoxy)phenyl]-5-methyl-5,6-dihydrophenanthridine-3,8-diamine

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Chemical Property of 6-[4-(2-fluoroethoxy)phenyl]-5-methyl-5,6-dihydrophenanthridine-3,8-diamine

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Technology Process of 6-[4-(2-fluoroethoxy)phenyl]-5-methyl-5,6-dihydrophenanthridine-3,8-diamine

There total 11 articles about 6-[4-(2-fluoroethoxy)phenyl]-5-methyl-5,6-dihydrophenanthridine-3,8-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1314081-12-3
di-tert-butyl {6-[4-(2-fluoroethoxy)phenyl]-5-methyl-5,6-dihydrophenanthridine-3,8-diyl}dicarbamate

: 1314081-13-4
6-[4-(2-fluoroethoxy)phenyl]-5-methyl-5,6-dihydrophenanthridine-3,8-diamine

Guidance literature:: With hydrogenchloride; water; In ethyl acetate; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/acschemneuro.7b00385

Reference yield:

: 1314081-04-3
di-tert-butyl [6-(4-hydroxyphenyl)phenanthridine-3,8-diyl]dicarbamate

: 1314081-13-4
6-[4-(2-fluoroethoxy)phenyl]-5-methyl-5,6-dihydrophenanthridine-3,8-diamine

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / acetone

2: tetrahydrofuran

3: sodium cyanoborohydride

4: hydrogenchloride / ethyl acetate

With hydrogenchloride; sodium cyanoborohydride; potassium carbonate; In tetrahydrofuran; ethyl acetate; acetone;

Reference yield:

: 1314081-10-1
di-tert-butyl {6-[4-(2-fluoroethoxy)phenyl]phenanthridine-3,8-diyl}dicarbamate

: 1314081-13-4
6-[4-(2-fluoroethoxy)phenyl]-5-methyl-5,6-dihydrophenanthridine-3,8-diamine

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran

2: sodium cyanoborohydride

3: hydrogenchloride / ethyl acetate

With hydrogenchloride; sodium cyanoborohydride; In tetrahydrofuran; ethyl acetate;