di-tert-butyl {6-[4-(2-fluoroethoxy)phenyl]phenanthridine-3,8-diyl}dicarbamate

Base Information

Chemical Name:di-tert-butyl {6-[4-(2-fluoroethoxy)phenyl]phenanthridine-3,8-diyl}dicarbamate
CAS No.:1314081-10-1
Molecular Formula:C₃₁H₃₄FN₃O₅
Molecular Weight:547.626
Hs Code.:

Synonyms:di-tert-butyl {6-[4-(2-fluoroethoxy)phenyl]phenanthridine-3,8-diyl}dicarbamate

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Chemical Property of di-tert-butyl {6-[4-(2-fluoroethoxy)phenyl]phenanthridine-3,8-diyl}dicarbamate

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Technology Process of di-tert-butyl {6-[4-(2-fluoroethoxy)phenyl]phenanthridine-3,8-diyl}dicarbamate

There total 9 articles about di-tert-butyl {6-[4-(2-fluoroethoxy)phenyl]phenanthridine-3,8-diyl}dicarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1314081-04-3
di-tert-butyl [6-(4-hydroxyphenyl)phenanthridine-3,8-diyl]dicarbamate

: 383-50-6
2-fluoroethyl tosylate

: 1314081-10-1
di-tert-butyl {6-[4-(2-fluoroethoxy)phenyl]phenanthridine-3,8-diyl}dicarbamate

Guidance literature:: With potassium carbonate; In acetonitrile; at 80 ℃;
DOI:10.1021/acschemneuro.7b00385

Reference yield:

: 762-49-2
2-fluoroethyl bromide

: 1314081-04-3
di-tert-butyl [6-(4-hydroxyphenyl)phenanthridine-3,8-diyl]dicarbamate

: 1314081-10-1
di-tert-butyl {6-[4-(2-fluoroethoxy)phenyl]phenanthridine-3,8-diyl}dicarbamate

Guidance literature:: With potassium carbonate; In acetone;

Reference yield:

: 100-07-2
4-methoxy-benzoyl chloride

: 1314081-10-1
di-tert-butyl {6-[4-(2-fluoroethoxy)phenyl]phenanthridine-3,8-diyl}dicarbamate

Guidance literature:: Multi-step reaction with 7 steps

1: chlorobenzene / Reflux

2: ammonium formate / 20 % Pd(OH)2/C

4: trichlorophosphate

5: hydrogen bromide / water

7: potassium carbonate / acetone

With hydrogen bromide; ammonium formate; potassium carbonate; trichlorophosphate; 20 % Pd(OH)2/C; In water; chlorobenzene; acetone;