N⁵,1-Dibenzoyl-N⁵-(phenylsulfonyl)-5-amino-7-(benzyloxy)-3-methylindole

Base Information

Chemical Name:N⁵,1-Dibenzoyl-N⁵-(phenylsulfonyl)-5-amino-7-(benzyloxy)-3-methylindole
CAS No.:124400-38-0
Molecular Formula:C₃₆H₂₈N₂O₅S
Molecular Weight:600.695
Hs Code.:

N<sup>5</sup>,1-Dibenzoyl-N<sup>5</sup>-(phenylsulfonyl)-5-amino-7-(benzyloxy)-3-methylindole

Synonyms:N⁵,1-Dibenzoyl-N⁵-(phenylsulfonyl)-5-amino-7-(benzyloxy)-3-methylindole

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Chemical Property of N⁵,1-Dibenzoyl-N⁵-(phenylsulfonyl)-5-amino-7-(benzyloxy)-3-methylindole

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Technology Process of N⁵,1-Dibenzoyl-N⁵-(phenylsulfonyl)-5-amino-7-(benzyloxy)-3-methylindole

There total 4 articles about N⁵,1-Dibenzoyl-N⁵-(phenylsulfonyl)-5-amino-7-(benzyloxy)-3-methylindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 112764-63-3
N⁵-(Phenylsulfonyl)-5-amino-1-benzoyl-7-(benzyloxy)-3-methylindole

: 98-88-4
benzoyl chloride

: 124400-38-0
N⁵,1-Dibenzoyl-N⁵-(phenylsulfonyl)-5-amino-7-(benzyloxy)-3-methylindole

Guidance literature:: With potassium carbonate; In tetrahydrofuran; at 25 ℃; for 12h;
DOI:10.1021/jo00291a059

Reference yield:

: 114996-60-0
N¹,N⁴-Dibenzoyl-2-(benzyloxy)-p-benzoquinone Diimine

: 124400-38-0
N⁵,1-Dibenzoyl-N⁵-(phenylsulfonyl)-5-amino-7-(benzyloxy)-3-methylindole

Guidance literature:: Multi-step reaction with 2 steps

1: 2) 10percent aq. HCl / 1) CH₂Cl₂, 25 deg C, 8 h, 2) THF, 25 deg C, 24 h

2: 1) potassium hydride / 1) THF, 25 deg C, 0.5 h, 2) 50 deg C, 12 h

With hydrogenchloride; potassium hydride;
DOI:10.1021/jo00291a059

Reference yield:

: 124400-65-3
O-Benzyl-N²,N⁵-dibenzoyl-2,5-diamino-3-<3-(3-methyl-1-propenyl)>phenol

: 124400-38-0
N⁵,1-Dibenzoyl-N⁵-(phenylsulfonyl)-5-amino-7-(benzyloxy)-3-methylindole

Guidance literature:: Multi-step reaction with 2 steps

1: 1) OsO₄, NaIO₄, 2) H₂SO₄ (10percent in CH₂Cl₂) / 1) acetone, water, 25 deg C, 2) CH₂Cl₂, 25 deg C

2: 1) potassium hydride / 1) THF, 25 deg C, 0.5 h, 2) 50 deg C, 12 h

With sodium periodate; osmium(VIII) oxide; sulfuric acid; potassium hydride;
DOI:10.1021/jo00291a059