2-hydoxy-3-methyl-(S)-pyrrolidine-2-carboxylate-5-methylbenzaldehyde methyl ester

Base Information

Chemical Name:2-hydoxy-3-methyl-(S)-pyrrolidine-2-carboxylate-5-methylbenzaldehyde methyl ester
CAS No.:1393553-56-4
Molecular Formula:C₁₅H₁₉NO₄
Molecular Weight:277.32
Hs Code.:

Synonyms:2-hydoxy-3-methyl-(S)-pyrrolidine-2-carboxylate-5-methylbenzaldehyde methyl ester

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Chemical Property of 2-hydoxy-3-methyl-(S)-pyrrolidine-2-carboxylate-5-methylbenzaldehyde methyl ester

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Technology Process of 2-hydoxy-3-methyl-(S)-pyrrolidine-2-carboxylate-5-methylbenzaldehyde methyl ester

There total 1 articles about 2-hydoxy-3-methyl-(S)-pyrrolidine-2-carboxylate-5-methylbenzaldehyde methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 192819-68-4
3-chloromethyl-5-methylsalicylaldehyde

: 2133-40-6
L-proline methyl ester monohydrochloride

: 1393553-56-4
2-hydoxy-3-methyl-(S)-pyrrolidine-2-carboxylate-5-methylbenzaldehyde methyl ester

Guidance literature:: With triethylamine; In tetrahydrofuran; dichloromethane; at 20 ℃;
DOI:10.1021/ic300967j

Reference yield: 41.0%

: 1393553-56-4
2-hydoxy-3-methyl-(S)-pyrrolidine-2-carboxylate-5-methylbenzaldehyde methyl ester

: 79-19-6
thiosemicarbazide

: L-Pro-STSC

Guidance literature:: In ethanol; water; at 70 - 75 ℃; for 75h;
DOI:10.1021/ic300967j

Reference yield:

: 1393553-56-4
2-hydoxy-3-methyl-(S)-pyrrolidine-2-carboxylate-5-methylbenzaldehyde methyl ester

: 2-hydoxy-3-methyl-(S)-pyrrolidine-2-carboxylate-5-methylbenzaldehyde

Guidance literature:: 2-hydoxy-3-methyl-(S)-pyrrolidine-2-carboxylate-5-methylbenzaldehyde methyl ester; With sodium hydroxide; In water;

With hydrogenchloride; In water;
DOI:10.1039/c7dt02360j