{3-[3,5-bis-(3-tert-butoxycarbonylamino-propyl)-phenyl]-propyl}-carbamic acid tert-butyl ester

Base Information

Chemical Name:{3-[3,5-bis-(3-tert-butoxycarbonylamino-propyl)-phenyl]-propyl}-carbamic acid tert-butyl ester
CAS No.:606126-69-6
Molecular Formula:C₃₀H₅₁N₃O₆
Molecular Weight:549.751
Hs Code.:

{3-[3,5-bis-(3-<i>tert</i>-butoxycarbonylamino-propyl)-phenyl]-propyl}-carbamic acid <i>tert</i>-butyl ester

Synonyms:{3-[3,5-bis-(3-tert-butoxycarbonylamino-propyl)-phenyl]-propyl}-carbamic acid tert-butyl ester

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Chemical Property of {3-[3,5-bis-(3-tert-butoxycarbonylamino-propyl)-phenyl]-propyl}-carbamic acid tert-butyl ester

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Technology Process of {3-[3,5-bis-(3-tert-butoxycarbonylamino-propyl)-phenyl]-propyl}-carbamic acid tert-butyl ester

There total 1 articles about {3-[3,5-bis-(3-tert-butoxycarbonylamino-propyl)-phenyl]-propyl}-carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 626-39-1
1,3,5-trisbromobenzene

: 78888-18-3
N-tert-butoxycarbonylprop-2-en-1-amine

: 606126-69-6
{3-[3,5-bis-(3-tert-butoxycarbonylamino-propyl)-phenyl]-propyl}-carbamic acid tert-butyl ester

Guidance literature:: N-tert-butoxycarbonylprop-2-en-1-amine; With 9-borabicyclononane; In toluene; at 20 ℃; for 12h;

1,3,5-trisbromobenzene; With potassium hydroxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; at 50 ℃; for 24h; Further stages.;
DOI:10.1002/chem.200305386

Reference yield: 95.6%

: 606126-69-6
{3-[3,5-bis-(3-tert-butoxycarbonylamino-propyl)-phenyl]-propyl}-carbamic acid tert-butyl ester

: 1,3,5-tris(3-aminopropyl)benzene

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; at 20 ℃; for 12h;
DOI:10.1002/chem.200305386

Reference yield:

: 606126-69-6
{3-[3,5-bis-(3-tert-butoxycarbonylamino-propyl)-phenyl]-propyl}-carbamic acid tert-butyl ester

: 2,3-diamino-N-(3-{3,5-bis-[3-(2,3-diamino-propionylamino)-propyl]-phenyl}-propyl)-propionamide; compound with trifluoro-acetic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: 95.6 percent / aq. HCl / tetrahydrofuran / 12 h / 20 °C

2.1: N-ethyl-diisopropylamine; O-(1H-benzotriazole-1-yl)-N,N,N',N'-tetramethyluronium BF₄ / dimethylformamide; CH₂Cl₂ / 0.75 h / -20 - 20 °C

2.2: 80 percent / N-ethyl-diisopropylamine / dimethylformamide; methanol; CH₂Cl₂ / 12 h / -20 - 20 °C

3.1: 99.8 percent / CH₂Cl₂ / 1 h / 20 °C

With hydrogenchloride; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.200305386