2-(dibutoxymethyl)-5-(phenoxymethyl)furan

Base Information

• Chemical Name: 2-(dibutoxymethyl)-5-(phenoxymethyl)furan
• CAS No.: 1531604-75-7
• Molecular Formula: C₂₀H₂₈O₄
• Molecular Weight: 332.44
• Mol file: 1531604-75-7.mol

Synonyms:2-(dibutoxymethyl)-5-(phenoxymethyl)furan

Chemical Property of 2-(dibutoxymethyl)-5-(phenoxymethyl)furan

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 2-(dibutoxymethyl)-5-(phenoxymethyl)furan

There total 2 articles about 2-(dibutoxymethyl)-5-(phenoxymethyl)furan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

2-(chloromethyl)-5-(dibutoxymethyl)furan (126080-78-2) + phenol (108-95-2,27073-41-2) → 2-(dibutoxymethyl)-5-(phenoxymethyl)furan (1531604-75-7)

Guidance literature:

With potassium carbonate; In dimethyl sulfoxide; at 50 ℃; for 5h; Inert atmosphere;

DOI:10.1021/jf4045843 DOI:10.1021/jf4045843

Reference yield:

5-chloromethylfurfural (1623-88-7) → 2-(dibutoxymethyl)-5-(phenoxymethyl)furan (1531604-75-7)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrogenchloride / water / Cooling with ice

2: potassium carbonate / dimethyl sulfoxide / 5 h / 50 °C / Inert atmosphere

With hydrogenchloride; potassium carbonate; In water; dimethyl sulfoxide;

DOI:10.1021/jf4045843

Reference yield: 99.0%

2-(dibutoxymethyl)-5-(phenoxymethyl)furan (1531604-75-7) → 5-(phenoxymethyl)-2-furan carbaldehyde (685904-18-1)

Guidance literature:

With hydrogenchloride; In water; for 2h;

DOI:10.1021/jf4045843 DOI:10.1021/jf4045843

upstream raw materials:

2-(chloromethyl)-5-(dibutoxymethyl)furan

phenol

5-chloromethylfurfural

Downstream raw materials:

5-(phenoxymethyl)-2-furan carbaldehyde

2-(hydroxymethyl)-5-(phenoxymethyl)furan

(±)-cis- and (±)-trans-[5-(phenoxymethyl)furan-2-yl]methyl-2,2-dimethyl-3-(2-methylprop-1-en-1-yl)-cyclopropane-1-carboxylate