7-phenyl-5,6-dihydrobenzacridine

Base Information

• Chemical Name: 7-phenyl-5,6-dihydrobenzacridine
• CAS No.: 79039-74-0
• Molecular Formula: C₂₃H₁₇N
• Molecular Weight: 307.395
• Mol file: 79039-74-0.mol

Synonyms:7-phenyl-5,6-dihydrobenzacridine

Chemical Property of 7-phenyl-5,6-dihydrobenzacridine

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 7-phenyl-5,6-dihydrobenzacridine

There total 9 articles about 7-phenyl-5,6-dihydrobenzacridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

3,4-dihydronaphthalene-1(2H)-one (529-34-0) + (2-aminophenyl)(phenyl)methanone (2835-77-0) → 7-phenyl-5,6-dihydrobenzacridine (79039-74-0)

Guidance literature:

With ammonium cerium (IV) nitrate; at 60 ℃; for 0.5h; Ionic liquid;

DOI:10.3987/COM-09-11865

Reference yield: 85.0%

(5,6-dihydrobenzo[c]acridin-7-yl)(phenyl)methanone → 7-phenyl-5,6-dihydrobenzacridine (79039-74-0)

Guidance literature:

With trifluorormethanesulfonic acid; [bis(acetoxy)iodo]benzene; oxygen; In dimethyl sulfoxide; at 110 ℃; for 14h; Sealed tube;

DOI:10.1021/acs.orglett.0c00304

Reference yield: 78.0%

2-phenylethynylaniline (13141-38-3) + 3,4-dihydronaphthalene-1(2H)-one (529-34-0) → 7-phenyl-5,6-dihydrobenzacridine (79039-74-0)

Guidance literature:

With trifluorormethanesulfonic acid; [bis(acetoxy)iodo]benzene; oxygen; In dimethyl sulfoxide; at 110 ℃; for 48h; Reagent/catalyst; Mechanism; Sealed tube;

DOI:10.1021/acs.orglett.0c00304

upstream raw materials:

1-tetralone oxime

(2-aminophenyl)(phenyl)methanone

3,4-dihydronaphthalene-1(2H)-one

2-phenylethynylaniline