t-butyl 9-(3,4-dimethoxyphenyl)-6,7-dimethoxy-1-oxo-1,3-dihydronaphtho[2,3-c]furan-4-yl carbonate

Base Information

Chemical Name:t-butyl 9-(3,4-dimethoxyphenyl)-6,7-dimethoxy-1-oxo-1,3-dihydronaphtho[2,3-c]furan-4-yl carbonate
CAS No.:1621253-12-0
Molecular Formula:C₂₇H₂₈O₉
Molecular Weight:496.514
Hs Code.:

Synonyms:t-butyl 9-(3,4-dimethoxyphenyl)-6,7-dimethoxy-1-oxo-1,3-dihydronaphtho[2,3-c]furan-4-yl carbonate

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Chemical Property of t-butyl 9-(3,4-dimethoxyphenyl)-6,7-dimethoxy-1-oxo-1,3-dihydronaphtho[2,3-c]furan-4-yl carbonate

Chemical Property:

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Technology Process of t-butyl 9-(3,4-dimethoxyphenyl)-6,7-dimethoxy-1-oxo-1,3-dihydronaphtho[2,3-c]furan-4-yl carbonate

There total 1 articles about t-butyl 9-(3,4-dimethoxyphenyl)-6,7-dimethoxy-1-oxo-1,3-dihydronaphtho[2,3-c]furan-4-yl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1621253-12-0
t-butyl 9-(3,4-dimethoxyphenyl)-6,7-dimethoxy-1-oxo-1,3-dihydronaphtho[2,3-c]furan-4-yl carbonate

Guidance literature:: With palladium diacetate; caesium carbonate; tricyclohexylphosphine; In 1,4-dioxane; water; at 80 ℃; for 17h;

Reference yield: 90.0%

: 1621253-12-0
t-butyl 9-(3,4-dimethoxyphenyl)-6,7-dimethoxy-1-oxo-1,3-dihydronaphtho[2,3-c]furan-4-yl carbonate

: 104757-12-2
1-(3,4-dimethoxyphenyl)-4-hydroxy-3-(hydroxymethyl)-6,7-dimethoxynaphthalene-2-carboxylic acid lactone

Guidance literature:: With piperidine; In dichloromethane; at 0 - 25 ℃; for 5h;

Reference yield:

: 1621253-12-0
t-butyl 9-(3,4-dimethoxyphenyl)-6,7-dimethoxy-1-oxo-1,3-dihydronaphtho[2,3-c]furan-4-yl carbonate

: 9-(3,4-dimethoxyphenyl)-4,6,7-trimethoxynaphtho[2,3-c]furan-1(3H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: piperidine / dichloromethane / 5 h / 0 - 25 °C

2: potassium carbonate / N,N-dimethyl-formamide / 2 h / 0 - 40 °C

With piperidine; potassium carbonate; In dichloromethane; N,N-dimethyl-formamide;