C₂₄H₂₂N₂O₄

Base Information

Chemical Name:C₂₄H₂₂N₂O₄
CAS No.:1399266-39-7
Molecular Formula:C₂₄H₂₂N₂O₄
Molecular Weight:402.45
Hs Code.:

C<sub>24</sub>H<sub>22</sub>N<sub>2</sub>O<sub>4</sub>

Synonyms:C₂₄H₂₂N₂O₄

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Chemical Property of C₂₄H₂₂N₂O₄

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Technology Process of C₂₄H₂₂N₂O₄

There total 8 articles about C₂₄H₂₂N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1399266-36-4
C₃₂H₂₄N₂O₆

: 1399266-39-7
C₂₄H₂₂N₂O₄

Guidance literature:: C₃₂H₂₄N₂O₆; In tetrahydrofuran; at 0 ℃; for 0.25h;

With methylhydrazine; In tetrahydrofuran; at 0 - 22 ℃; for 3h;
DOI:10.1039/c2ob26077h

Reference yield:

: 65-49-6
4-Aminosalicylic acid

: 1399266-39-7
C₂₄H₂₂N₂O₄

Guidance literature:: Multi-step reaction with 8 steps

1.1: sulfuric acid / 22 °C

2.1: acetic acid / 22 h / 118 °C / Inert atmosphere

3.1: potassium carbonate / N,N-dimethyl-formamide / 24 h / 22 °C / Inert atmosphere

4.1: potassium hydroxide; water / methanol / 18.5 h / 22 °C

5.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 3.5 h / 22 °C / Inert atmosphere

6.1: N-ethyl-N,N-diisopropylamine / dichloromethane / -78 - 22 °C / Inert atmosphere

7.1: diethylamino-sulfur trifluoride / dichloromethane / 5 h / -78 °C / Inert atmosphere

7.2: -78 - 22 °C

8.1: tetrahydrofuran / 0.25 h / 0 °C

8.2: 3 h / 0 - 22 °C

With oxalyl dichloride; diethylamino-sulfur trifluoride; sulfuric acid; water; potassium carbonate; N-ethyl-N,N-diisopropylamine; N,N-dimethyl-formamide; potassium hydroxide; In tetrahydrofuran; methanol; dichloromethane; acetic acid; N,N-dimethyl-formamide;
DOI:10.1039/c2ob26077h

Reference yield:

: 1399266-27-3
C₂₃H₁₇NO₅

: 1399266-39-7
C₂₄H₂₂N₂O₄

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium hydroxide; water / methanol / 18.5 h / 22 °C

2.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 3.5 h / 22 °C / Inert atmosphere

3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / -78 - 22 °C / Inert atmosphere

4.1: diethylamino-sulfur trifluoride / dichloromethane / 5 h / -78 °C / Inert atmosphere

4.2: -78 - 22 °C

5.1: tetrahydrofuran / 0.25 h / 0 °C

5.2: 3 h / 0 - 22 °C

With oxalyl dichloride; diethylamino-sulfur trifluoride; water; N-ethyl-N,N-diisopropylamine; N,N-dimethyl-formamide; potassium hydroxide; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1039/c2ob26077h