methyl N-[(2,6-dimethyl-3-pyridinyl)methylidene]-D-alloisoleucine

Base Information

Chemical Name:methyl N-[(2,6-dimethyl-3-pyridinyl)methylidene]-D-alloisoleucine
CAS No.:1299957-27-9
Molecular Formula:C₁₅H₂₂N₂O₂
Molecular Weight:262.352
Hs Code.:

Synonyms:methyl N-[(2,6-dimethyl-3-pyridinyl)methylidene]-D-alloisoleucine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl N-[(2,6-dimethyl-3-pyridinyl)methylidene]-D-alloisoleucine

Chemical Property:

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Technology Process of methyl N-[(2,6-dimethyl-3-pyridinyl)methylidene]-D-alloisoleucine

There total 1 articles about methyl N-[(2,6-dimethyl-3-pyridinyl)methylidene]-D-alloisoleucine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2577-46-0,18869-44-8,42271-58-9,81084-74-4,107998-45-8,118878-53-8
D-allo-isoleucine methyl ester

: 650141-20-1
2,6-dimethylpyridine-3-carboxaldehyde

: 1299957-27-9
methyl N-[(2,6-dimethyl-3-pyridinyl)methylidene]-D-alloisoleucine

Guidance literature:: In methanol; 2,2,2-trifluoroethanol; at 40 ℃;

Reference yield:

: 554448-74-7
(2R)-2,3-dihydro-1H-inden-2-yl({[(phenylmethyl)oxy]carbonyl}amino)ethanoic acid

: 1299957-27-9
methyl N-[(2,6-dimethyl-3-pyridinyl)methylidene]-D-alloisoleucine

: 86652-64-4
1-benzyloxy-2-isocyanobenzene

: 872599-76-3
methyl N-[(2R)-2-(2,3-dihydro-1H-inden-2-yl)-2-({[(phenylmethyl)oxy]-carbonyl}amino)acetyl]-N-[1-(2,6-dimethyl-3-pyridinyl)-2-oxo-2-({2-[(phenylmethyl)oxy]phenyl}amino)ethyl]-D-alloisoleucinate

Guidance literature:: In methanol; 2,2,2-trifluoroethanol; at 40 ℃;

Reference yield:

: 1299957-27-9
methyl N-[(2,6-dimethyl-3-pyridinyl)methylidene]-D-alloisoleucine

: 2-{(3R,6R)-3-(2,3-dihydro-1H-inden-2-yl)-6-[(1S)-1-methylpropyl]-2,5-dioxo-1-piperazinyl}-2-(2,6-dimethyl-3-pyridinyl)-N-(2-hydroxyphenyl)acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 2,2,2-trifluoroethanol; methanol / 40 °C

2: hydrogen / palladium on carbon / acetic acid; 2,2,2-trifluoroethanol; methanol / 50 °C

With hydrogen; palladium on carbon; In methanol; 2,2,2-trifluoroethanol; acetic acid;