2-methoxy-5-nitroisophthalic acid diallyl ester

Base Information

Chemical Name:2-methoxy-5-nitroisophthalic acid diallyl ester
CAS No.:916177-63-4
Molecular Formula:C₁₅H₁₅NO₇
Molecular Weight:321.287
Hs Code.:

Synonyms:2-methoxy-5-nitroisophthalic acid diallyl ester

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Chemical Property of 2-methoxy-5-nitroisophthalic acid diallyl ester

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Technology Process of 2-methoxy-5-nitroisophthalic acid diallyl ester

There total 1 articles about 2-methoxy-5-nitroisophthalic acid diallyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 140362-00-1
2-methoxy-5-nitro-1,3-benzenedicarboxylic acid chloride

: 107-18-6
allyl alcohol

: 916177-63-4
2-methoxy-5-nitroisophthalic acid diallyl ester

Guidance literature:: With pyridine; In tetrahydrofuran; for 2h;
DOI:10.1021/ja066126z

Reference yield: 92.0%

: 916177-63-4
2-methoxy-5-nitroisophthalic acid diallyl ester

: 886758-03-8
5-amino-2-methoxyisophthalic acid diallyl ester

Guidance literature:: With tin(ll) chloride; In methanol; ethyl acetate; for 2h; Heating;
DOI:10.1021/ja066126z

Reference yield:

: 916177-63-4
2-methoxy-5-nitroisophthalic acid diallyl ester

: 916177-72-5
C₃₁H₂₇N₅O₇

Guidance literature:: Multi-step reaction with 6 steps

1: 92 percent / SnCl₂ / methanol; ethyl acetate / 2 h / Heating

2: 90 percent / acetic acid / 12 h / 80 °C

3: 98 percent / N,N-dimethylbarbituric acid / Pd₂(dba)3*CHCl₃; triphenylphosphine / tetrahydrofuran / 0.5 h

4: oxalyl chloride; DMF / tetrahydrofuran / 3 h / 20 °C

5: 85 percent / pyridine; 4-(dimethylamino)pyridine; 4 Angstroem molecular sieves / CHCl₃ / 3 h / 20 °C

6: 94 percent / HF*pyridine / 3 h / 20 °C

With pyridine; dmap; oxalyl dichloride; 1,3-dimethylbarbituric acid; 4 A molecular sieve; pyridine hydrogenfluoride; N,N-dimethyl-formamide; tin(ll) chloride; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; triphenylphosphine; In tetrahydrofuran; methanol; chloroform; acetic acid; ethyl acetate;
DOI:10.1021/ja066126z