N-benzyl-N-{2-[3-(tert-butyldimethylsilyloxy)prop-1-en-2-yl]phenyl}-1-cyanoformamide

Base Information

Chemical Name:N-benzyl-N-{2-[3-(tert-butyldimethylsilyloxy)prop-1-en-2-yl]phenyl}-1-cyanoformamide
CAS No.:1042150-58-2
Molecular Formula:C₂₄H₃₀N₂O₂Si
Molecular Weight:406.6
Hs Code.:

Synonyms:N-benzyl-N-{2-[3-(tert-butyldimethylsilyloxy)prop-1-en-2-yl]phenyl}-1-cyanoformamide

Suppliers and Price of N-benzyl-N-{2-[3-(tert-butyldimethylsilyloxy)prop-1-en-2-yl]phenyl}-1-cyanoformamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-benzyl-N-{2-[3-(tert-butyldimethylsilyloxy)prop-1-en-2-yl]phenyl}-1-cyanoformamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-benzyl-N-{2-[3-(tert-butyldimethylsilyloxy)prop-1-en-2-yl]phenyl}-1-cyanoformamide

There total 1 articles about N-benzyl-N-{2-[3-(tert-butyldimethylsilyloxy)prop-1-en-2-yl]phenyl}-1-cyanoformamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1115-12-4
carbonyl cyanide

: 1042150-51-5
N-benzyl-2-[3-(tert-butyldimethylsilyloxy)prop-1-en-2-yl]aniline

: 1042150-58-2
N-benzyl-N-{2-[3-(tert-butyldimethylsilyloxy)prop-1-en-2-yl]phenyl}-1-cyanoformamide

Guidance literature:: In diethyl ether; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol902949d

Reference yield: 90.0%

: 1042150-58-2
N-benzyl-N-{2-[3-(tert-butyldimethylsilyloxy)prop-1-en-2-yl]phenyl}-1-cyanoformamide

: 1042150-65-1
C₂₄H₃₀N₂O₂Si

Guidance literature:: With triethylamine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; tri tert-butylphosphoniumtetrafluoroborate; In 5,5-dimethyl-1,3-cyclohexadiene; at 130 ℃; for 6h; Inert atmosphere;
DOI:10.1016/j.tet.2010.01.073

Reference yield: 80.0%

: 1042150-58-2
N-benzyl-N-{2-[3-(tert-butyldimethylsilyloxy)prop-1-en-2-yl]phenyl}-1-cyanoformamide

: 1208117-63-8
(S)-2-(1-benzyl-3-((tert-butyldimethylsilyloxy)methyl)-2-oxo-indolin-3-yl)acetonitrile

Guidance literature:: With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; (R)-5,5’,6,6’,7,7’,8,8’-octahydro-1,1-binaphthylphosphinite diisopropylamidite; In tetrahydrofuran; at 100 ℃; for 24h; optical yield given as %ee; enantioselective reaction; Sealed vial; Inert atmosphere;
DOI:10.1016/j.tet.2010.02.096