{4-[7-bromo-5,5,10,10,15,15-hexahexyl-12-(4-hydroxymethyl-phenyl)-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluoren-2-yl]-phenyl}-methanol

Base Information

Chemical Name:{4-[7-bromo-5,5,10,10,15,15-hexahexyl-12-(4-hydroxymethyl-phenyl)-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluoren-2-yl]-phenyl}-methanol
CAS No.:912443-48-2
Molecular Formula:C₇₇H₁₀₁BrO₂
Molecular Weight:1138.55
Hs Code.:

{4-[7-bromo-5,5,10,10,15,15-hexahexyl-12-(4-hydroxymethyl-phenyl)-10,15-dihydro-5<i>H</i>-diindeno[1,2-<i>a</i>;1',2'-<i>c</i>]fluoren-2-yl]-phenyl}-methanol

Synonyms:{4-[7-bromo-5,5,10,10,15,15-hexahexyl-12-(4-hydroxymethyl-phenyl)-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluoren-2-yl]-phenyl}-methanol

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Chemical Property of {4-[7-bromo-5,5,10,10,15,15-hexahexyl-12-(4-hydroxymethyl-phenyl)-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluoren-2-yl]-phenyl}-methanol

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Technology Process of {4-[7-bromo-5,5,10,10,15,15-hexahexyl-12-(4-hydroxymethyl-phenyl)-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluoren-2-yl]-phenyl}-methanol

There total 3 articles about {4-[7-bromo-5,5,10,10,15,15-hexahexyl-12-(4-hydroxymethyl-phenyl)-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluoren-2-yl]-phenyl}-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: C₇₇H₉₇BrO₂

: 912443-48-2
{4-[7-bromo-5,5,10,10,15,15-hexahexyl-12-(4-hydroxymethyl-phenyl)-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluoren-2-yl]-phenyl}-methanol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; Heating;
DOI:10.1021/ol0616283

Reference yield:

: 87199-17-5
4-formylphenylboronic acid,

: 912443-48-2
{4-[7-bromo-5,5,10,10,15,15-hexahexyl-12-(4-hydroxymethyl-phenyl)-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluoren-2-yl]-phenyl}-methanol

Guidance literature:: Multi-step reaction with 2 steps

1: 23 percent / Na₂CO₃ / Pd(PPh₃)4 / tetrahydrofuran; H₂O / 10 h / Heating

2: 95 percent / lithium aluminum hydride / diethyl ether / Heating

With lithium aluminium tetrahydride; sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; diethyl ether; water; 1: Suzuki cross-coupling;
DOI:10.1021/ol0616283

Reference yield:

: 600172-86-9
2,7,12-tribromo-5,5',10,10',15,15'-hexahexyltruxene

: 912443-48-2
{4-[7-bromo-5,5,10,10,15,15-hexahexyl-12-(4-hydroxymethyl-phenyl)-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluoren-2-yl]-phenyl}-methanol

Guidance literature:: Multi-step reaction with 2 steps

1: 23 percent / Na₂CO₃ / Pd(PPh₃)4 / tetrahydrofuran; H₂O / 10 h / Heating

2: 95 percent / lithium aluminum hydride / diethyl ether / Heating

With lithium aluminium tetrahydride; sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; diethyl ether; water; 1: Suzuki cross-coupling;
DOI:10.1021/ol0616283