4,4'-(((1,4-phenylenebis(ethylazanediyl))bis(carbonyl))bis-(ethylazanediyl))dibenzoic acid

Base Information

Chemical Name:4,4'-(((1,4-phenylenebis(ethylazanediyl))bis(carbonyl))bis-(ethylazanediyl))dibenzoic acid
CAS No.:1584300-16-2
Molecular Formula:C₃₀H₃₄N₄O₆
Molecular Weight:546.623
Hs Code.:

Synonyms:4,4'-(((1,4-phenylenebis(ethylazanediyl))bis(carbonyl))bis-(ethylazanediyl))dibenzoic acid

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Chemical Property of 4,4'-(((1,4-phenylenebis(ethylazanediyl))bis(carbonyl))bis-(ethylazanediyl))dibenzoic acid

Chemical Property:

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Technology Process of 4,4'-(((1,4-phenylenebis(ethylazanediyl))bis(carbonyl))bis-(ethylazanediyl))dibenzoic acid

There total 4 articles about 4,4'-(((1,4-phenylenebis(ethylazanediyl))bis(carbonyl))bis-(ethylazanediyl))dibenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₄H₄₂N₄O₆

: 1584300-16-2
4,4'-(((1,4-phenylenebis(ethylazanediyl))bis(carbonyl))bis-(ethylazanediyl))dibenzoic acid

Guidance literature:: C₃₄H₄₂N₄O₆; With potassium hydroxide; In ethanol; water; for 24h; Reflux;

With hydrogenchloride; In ethanol; water;
DOI:10.1021/cg401754q

Reference yield:

: 104-49-4
1,4-diisocyanatobenzene

: 1584300-16-2
4,4'-(((1,4-phenylenebis(ethylazanediyl))bis(carbonyl))bis-(ethylazanediyl))dibenzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / N,N-dimethyl-formamide / 24 h / 90 °C

2: sodium hydride / dichloromethane / 24 h / 0 °C

3: potassium hydroxide / ethanol; water / 24 h / Reflux

With sodium hydride; triethylamine; potassium hydroxide; In ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/cg401754q

Reference yield:

: 1637325-42-8
C₂₆H₂₆N₄O₆

: 1584300-16-2
4,4'-(((1,4-phenylenebis(ethylazanediyl))bis(carbonyl))bis-(ethylazanediyl))dibenzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / dichloromethane / 24 h / 0 °C

2: potassium hydroxide / ethanol; water / 24 h / Reflux

With sodium hydride; potassium hydroxide; In ethanol; dichloromethane; water;
DOI:10.1021/cg401754q