4,4'-(((1,4-phenylenebis(ethylazanediyl))bis(carbonyl))bis-(ethylazanediyl))bis(N-methylbenzamide)

Base Information

Chemical Name:4,4'-(((1,4-phenylenebis(ethylazanediyl))bis(carbonyl))bis-(ethylazanediyl))bis(N-methylbenzamide)
CAS No.:1584812-46-3
Molecular Formula:C₃₂H₄₀N₆O₄
Molecular Weight:572.707
Hs Code.:

Synonyms:4,4'-(((1,4-phenylenebis(ethylazanediyl))bis(carbonyl))bis-(ethylazanediyl))bis(N-methylbenzamide)

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Chemical Property of 4,4'-(((1,4-phenylenebis(ethylazanediyl))bis(carbonyl))bis-(ethylazanediyl))bis(N-methylbenzamide)

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Technology Process of 4,4'-(((1,4-phenylenebis(ethylazanediyl))bis(carbonyl))bis-(ethylazanediyl))bis(N-methylbenzamide)

There total 5 articles about 4,4'-(((1,4-phenylenebis(ethylazanediyl))bis(carbonyl))bis-(ethylazanediyl))bis(N-methylbenzamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1584300-16-2
4,4'-(((1,4-phenylenebis(ethylazanediyl))bis(carbonyl))bis-(ethylazanediyl))dibenzoic acid

: 74-89-5
methylamine

: 1584812-46-3
4,4'-(((1,4-phenylenebis(ethylazanediyl))bis(carbonyl))bis-(ethylazanediyl))bis(N-methylbenzamide)

Guidance literature:: With 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride; In water; N,N-dimethyl-formamide; at 20 ℃; for 24h;
DOI:10.1021/cg401754q

Reference yield:

: C₃₄H₄₂N₄O₆

: 1584812-46-3
4,4'-(((1,4-phenylenebis(ethylazanediyl))bis(carbonyl))bis-(ethylazanediyl))bis(N-methylbenzamide)

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide / ethanol; water / 24 h / Reflux

2: 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride / N,N-dimethyl-formamide; water / 24 h / 20 °C

With 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride; potassium hydroxide; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1021/cg401754q

Reference yield:

: 1637325-42-8
C₂₆H₂₆N₄O₆

: 1584812-46-3
4,4'-(((1,4-phenylenebis(ethylazanediyl))bis(carbonyl))bis-(ethylazanediyl))bis(N-methylbenzamide)

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / dichloromethane / 24 h / 0 °C

2: potassium hydroxide / ethanol; water / 24 h / Reflux

3: 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride / N,N-dimethyl-formamide; water / 24 h / 20 °C

With sodium hydride; 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride; potassium hydroxide; In ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/cg401754q