{Pt₂(CCHC₆H₅)(CCC₆H₅)(P(C₂H₅)3)4}⁽¹⁺⁾*BF₄^(1-)={Pt₂(CCHC₆H₅)(CCC₆H₅)(P(C₂H₅)3)4}BF₄

Base Information

• Chemical Name: {Pt₂(CCHC₆H₅)(CCC₆H₅)(P(C₂H₅)3)4}⁽¹⁺⁾*BF₄^(1-)={Pt₂(CCHC₆H₅)(CCC₆H₅)(P(C₂H₅)3)4}BF₄
• CAS No.: 106357-37-3
• Molecular Formula: BF₄*C₄₀H₇₁P₄Pt₂
• Molecular Weight: 1152.86

Synonyms:{Pt₂(CCHC₆H₅)(CCC₆H₅)(P(C₂H₅)3)4}⁽¹⁺⁾*BF₄^(1-)={Pt₂(CCHC₆H₅)(CCC₆H₅)(P(C₂H₅)3)4}BF₄

Chemical Property of {Pt₂(CCHC₆H₅)(CCC₆H₅)(P(C₂H₅)3)4}⁽¹⁺⁾*BF₄^(1-)={Pt₂(CCHC₆H₅)(CCC₆H₅)(P(C₂H₅)3)4}BF₄

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Technology Process of {Pt₂(CCHC₆H₅)(CCC₆H₅)(P(C₂H₅)3)4}⁽¹⁺⁾*BF₄^(1-)={Pt₂(CCHC₆H₅)(CCC₆H₅)(P(C₂H₅)3)4}BF₄

There total 1 articles about {Pt₂(CCHC₆H₅)(CCC₆H₅)(P(C₂H₅)3)4}⁽¹⁺⁾*BF₄^(1-)={Pt₂(CCHC₆H₅)(CCC₆H₅)(P(C₂H₅)3)4}BF₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

{Pt2(CCHC6H5)(CCC6H5)(P(C2H5)3)4}(1+)*BF4(1-)={Pt2(CCHC6H5)(CCC6H5)(P(C2H5)3)4}BF4 (106357-35-1) → {Pt2(CCHC6H5)(CCC6H5)(P(C2H5)3)4}(1+)*BF4(1-)={Pt2(CCHC6H5)(CCC6H5)(P(C2H5)3)4}BF4 (106357-37-3)

Guidance literature:

In acetone; educt prepared from (PEt3)2Pt(CCPh)2 and HPt(PEt3)2(acetone)BF4 in acetone at 20°C under N2, left to stand for 4 days; not isolated, detected by NMR; Kinetics;

Reference yield: 75.0%

{Pt2(CCHC6H5)(CCC6H5)(P(C2H5)3)4}(1+)*BF4(1-)={Pt2(CCHC6H5)(CCC6H5)(P(C2H5)3)4}BF4 (106357-37-3) + thiophenol (108-98-5) → {Pt2(CCHC6H5)(CCC6H5)(P(C2H5)3)3(SC6H5)} (122236-08-2)

Guidance literature:

With n-C₄H₉Li; In tetrahydrofuran; under N2, addn. of thiophenol to soln. of n-C4H9Li in THF, 0°C, stirring, 10 min, addn. of thiophenolate soln. to soln. of tetrakis-Et3P complex, 25°C, stirring, 1 h; evapn. of solvent in vac., extg. residue with diethyl ether, filtering through neutral alumina, evapn. of solvent in vac., chromy. (neutral alumina/hexane), crystn. from THF/hexane (1:9) at -15°C; elem. anal.;

DOI:10.1021/om00112a025

Reference yield: 72.0%

{Pt2(CCHC6H5)(CCC6H5)(P(C2H5)3)4}(1+)*BF4(1-)={Pt2(CCHC6H5)(CCC6H5)(P(C2H5)3)4}BF4 (106357-37-3) + lithium bromide (7550-35-8) → {Pt2(CCHC6H5)(CCC6H5)(P(C2H5)3)3Br} (122236-06-0)

Guidance literature:

In tetrahydrofuran; under N2, 25°C, stirring, 3 h; evapn. of solvent in vac., extg. residue with diethyl ether, filtering through neutral alumina, evapn. of solvent in vac., recrystn. from THF/hexane (1:4) at -15°C; elem. anal.;

DOI:10.1021/om00112a025

upstream raw materials:

{Pt₂(CCHC₆H₅)(CCC₆H₅)(P(C₂H₅)3)4}⁽¹⁺⁾*BF₄^(1-)={Pt₂(CCHC₆H₅)(CCC₆H₅)(P(C₂H₅)3)4}BF₄

Downstream raw materials:

{Pt₂(CCHC₆H₅)(CCC₆H₅)(P(C₂H₅)3)3Br}

{Pt₂(CCHC₆H₅)(CCC₆H₅)(P(C₂H₅)3)3(NCS)}

{Pt₂(CCHC₆H₅)(CCC₆H₅)(P(C₂H₅)3)3(NCS)}

{Pt₂(CCHC₆H₅)(CCC₆H₅)(P(C₂H₅)3)3I}

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