2,2'-thiodibenzoic acid chloride

Base Information

• Chemical Name: 2,2'-thiodibenzoic acid chloride
• CAS No.: 100541-19-3
• Molecular Formula: C₁₄H₈Cl₂O₂S
• Molecular Weight: 311.188
• Mol file: 100541-19-3.mol

Synonyms:2,2'-thiodibenzoic acid chloride

Chemical Property of 2,2'-thiodibenzoic acid chloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,2'-thiodibenzoic acid chloride

There total 5 articles about 2,2'-thiodibenzoic acid chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

2,2'-thiodibenzoic acid (22219-02-9) → 2,2'-thiodibenzoic acid chloride (100541-19-3)

Guidance literature:

With thionyl chloride;

Reference yield:

Thiosalicylic acid (147-93-3) → 2,2'-thiodibenzoic acid chloride (100541-19-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 96 percent / potassium carbonate, powdered copper / H₂O / 3 h / 130 - 140 °C

2: thionyl chloride / 5 h / 60 °C

With thionyl chloride; copper; potassium carbonate; In water;

DOI:10.1021/jo00321a020

Reference yield:

2-bromobenzoic-acid (88-65-3) → 2,2'-thiodibenzoic acid chloride (100541-19-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 96 percent / potassium carbonate, powdered copper / H₂O / 3 h / 130 - 140 °C

2: thionyl chloride / 5 h / 60 °C

With thionyl chloride; copper; potassium carbonate; In water;

DOI:10.1021/jo00321a020

upstream raw materials:

2,2'-thiodibenzoic acid

Thiosalicylic acid

ortho-chlorobenzoic acid

2-bromobenzoic-acid

Downstream raw materials:

bis-[2-(piperidine-1-carbonyl)-phenyl]-sulfide

2,2'-Thiobenzoesaeure-dimethylester

2,2'-dicarbethoxydiphenyl sulfide

2,2'-sulfanediyl-di-benzoic acid diamide