iodure de (phenyl-2 ethyl)-1 dicarbamoyl-3,5 methyl-7 pyrrolo<2,3-b>pyridinium

Base Information

Chemical Name:iodure de (phenyl-2 ethyl)-1 dicarbamoyl-3,5 methyl-7 pyrrolo<2,3-b>pyridinium
CAS No.:125189-47-1
Molecular Formula:C₁₈H₁₉N₄O₂*I
Molecular Weight:450.279
Hs Code.:

Synonyms:iodure de (phenyl-2 ethyl)-1 dicarbamoyl-3,5 methyl-7 pyrrolo<2,3-b>pyridinium

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Chemical Property of iodure de (phenyl-2 ethyl)-1 dicarbamoyl-3,5 methyl-7 pyrrolo<2,3-b>pyridinium

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Technology Process of iodure de (phenyl-2 ethyl)-1 dicarbamoyl-3,5 methyl-7 pyrrolo<2,3-b>pyridinium

There total 3 articles about iodure de (phenyl-2 ethyl)-1 dicarbamoyl-3,5 methyl-7 pyrrolo<2,3-b>pyridinium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 125189-46-0
(phenyl-2 ethyl)-1 dicarbamoyl-3,5 pyrrolo<2,3-b>pyridine

: 74-88-4
methyl iodide

: 125189-47-1
iodure de (phenyl-2 ethyl)-1 dicarbamoyl-3,5 methyl-7 pyrrolo<2,3-b>pyridinium

Guidance literature:: In N,N-dimethyl-formamide; for 72h; Heating;
DOI:10.1002/jhet.5570260424

Reference yield:

: 125189-45-9
1-Phenethyl-1H-pyrrolo[2,3-b]pyridine-3,5-dicarboxylic acid

: 125189-47-1
iodure de (phenyl-2 ethyl)-1 dicarbamoyl-3,5 methyl-7 pyrrolo<2,3-b>pyridinium

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) SOCl₂, 2.) NH₃ gas / 1.) reflux, 12 h, 2.) dichloromethane, 5 deg C, 10 min

2: 80 percent / dimethylformamide / 72 h / Heating

With thionyl chloride; ammonia; In N,N-dimethyl-formamide;
DOI:10.1002/jhet.5570260424

Reference yield:

: 125189-43-7
(phenyl-2 ethyl)-1 dicyano-3,5 pyrrolo<2,3-b>pyridine

: 125189-47-1
iodure de (phenyl-2 ethyl)-1 dicarbamoyl-3,5 methyl-7 pyrrolo<2,3-b>pyridinium

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / NaOH / ethanol; H₂O / 24 h / 80 °C

2: 1.) SOCl₂, 2.) NH₃ gas / 1.) reflux, 12 h, 2.) dichloromethane, 5 deg C, 10 min

3: 80 percent / dimethylformamide / 72 h / Heating

With sodium hydroxide; thionyl chloride; ammonia; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1002/jhet.5570260424