Technology Process of C38H43BF2N3P
There total 5 articles about C38H43BF2N3P which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
2,4-dimethyl-3-ethyl-pyrrole; C22H22NOP;
With
trifluoroacetic acid;
In
dichloromethane;
at 20 ℃;
for 1.5h;
Inert atmosphere;
With
2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
dichloromethane;
for 0.75h;
Inert atmosphere;
boron trifluoride diethyl etherate;
With
N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
for 1h;
Inert atmosphere;
DOI:10.1021/ic400383t
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: tetrachloromethane; triphenylphosphine / dichloromethane / 20 °C
2.1: tetrahydrofuran / 20 °C / Inert atmosphere
3.1: n-butyllithium / tetrahydrofuran / 0.75 h / -78 °C
3.2: -78 - 20 °C
4.1: trifluoroacetic acid / dichloromethane / 1.5 h / 20 °C / Inert atmosphere
4.2: 0.75 h / Inert atmosphere
4.3: 1 h / Inert atmosphere
With
tetrachloromethane; n-butyllithium; triphenylphosphine; trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane;
1.1: |Appel Halogenation;
DOI:10.1021/ic400383t
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: N-Bromosuccinimide / tetrachloromethane / 20 °C
2.1: tetrachloromethane; triphenylphosphine / dichloromethane / 20 °C
3.1: tetrahydrofuran / 20 °C / Inert atmosphere
4.1: n-butyllithium / tetrahydrofuran / 0.75 h / -78 °C
4.2: -78 - 20 °C
5.1: trifluoroacetic acid / dichloromethane / 1.5 h / 20 °C / Inert atmosphere
5.2: 0.75 h / Inert atmosphere
5.3: 1 h / Inert atmosphere
With
tetrachloromethane; N-Bromosuccinimide; n-butyllithium; triphenylphosphine; trifluoroacetic acid;
In
tetrahydrofuran; tetrachloromethane; dichloromethane;
2.1: |Appel Halogenation;
DOI:10.1021/ic400383t
