5-carboxypentyl 4-O-(2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranosyl)-3-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-2-acetamido-6-O-benzyl-2-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:5-carboxypentyl 4-O-(2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranosyl)-3-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-2-acetamido-6-O-benzyl-2-deoxy-β-D-glucopyranoside
CAS No.:1276117-50-0
Molecular Formula:C₆₃H₇₆N₂O₁₇
Molecular Weight:1133.3
Hs Code.:

5-carboxypentyl 4-O-(2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranosyl)-3-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-2-acetamido-6-O-benzyl-2-deoxy-β-D-glucopyranoside

Synonyms:5-carboxypentyl 4-O-(2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranosyl)-3-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-2-acetamido-6-O-benzyl-2-deoxy-β-D-glucopyranoside

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Chemical Property of 5-carboxypentyl 4-O-(2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranosyl)-3-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-2-acetamido-6-O-benzyl-2-deoxy-β-D-glucopyranoside

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Technology Process of 5-carboxypentyl 4-O-(2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranosyl)-3-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-2-acetamido-6-O-benzyl-2-deoxy-β-D-glucopyranoside

There total 2 articles about 5-carboxypentyl 4-O-(2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranosyl)-3-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-2-acetamido-6-O-benzyl-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1276117-49-7
5-(carboxyethyl)pentyl 4-O-(2-acetamido-3-O-acetyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranosyl)-3-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-2-acetamido-6-O-benzyl-2-deoxy-β-D-glucopyranoside

: 1276117-50-0
5-carboxypentyl 4-O-(2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranosyl)-3-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-2-acetamido-6-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: 5-(carboxyethyl)pentyl 4-O-(2-acetamido-3-O-acetyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranosyl)-3-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-2-acetamido-6-O-benzyl-2-deoxy-β-D-glucopyranoside; With water; sodium hydroxide; In tetrahydrofuran; at 75 ℃;

In tetrahydrofuran; water; at 20 ℃;
DOI:10.1016/j.bmc.2010.12.001

Reference yield:

: C₆₃H₇₈N₂O₁₆

: 1276117-50-0
5-carboxypentyl 4-O-(2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranosyl)-3-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-2-acetamido-6-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine / 20 °C / Inert atmosphere

2.1: water; sodium hydroxide / tetrahydrofuran / 75 °C

2.2: IR 120 H+ / 20 °C

With pyridine; water; sodium hydroxide; In tetrahydrofuran;
DOI:10.1016/j.bmc.2010.12.001

Reference yield: 54.0%

: 1276117-50-0
5-carboxypentyl 4-O-(2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranosyl)-3-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-2-acetamido-6-O-benzyl-2-deoxy-β-D-glucopyranoside

: 65953-56-2
N-(6-aminohexyl)-5-((3aS,4S,6aR)-3a,6a-dimethyl-2-oxohexahydro-1H-thieno[3,4-d] imidazol-4-yl)pentanamide

: 1276117-52-2
C₇₉H₁₀₄N₆O₁₈S

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 70 ℃; for 5h;
DOI:10.1016/j.bmc.2010.12.001