[3-[(4-chlorophenyl)sulfanyl]-1-(2-ethoxy-2-oxoethyl)-2-methyl-4,5,6,7-tetrahydro-1H-indol-4-ylidene]amino acetate

Base Information

Chemical Name:[3-[(4-chlorophenyl)sulfanyl]-1-(2-ethoxy-2-oxoethyl)-2-methyl-4,5,6,7-tetrahydro-1H-indol-4-ylidene]amino acetate
CAS No.:1260673-32-2
Molecular Formula:C₂₁H₂₃ClN₂O₄S
Molecular Weight:434.944
Hs Code.:

Synonyms:[3-[(4-chlorophenyl)sulfanyl]-1-(2-ethoxy-2-oxoethyl)-2-methyl-4,5,6,7-tetrahydro-1H-indol-4-ylidene]amino acetate

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Chemical Property of [3-[(4-chlorophenyl)sulfanyl]-1-(2-ethoxy-2-oxoethyl)-2-methyl-4,5,6,7-tetrahydro-1H-indol-4-ylidene]amino acetate

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Technology Process of [3-[(4-chlorophenyl)sulfanyl]-1-(2-ethoxy-2-oxoethyl)-2-methyl-4,5,6,7-tetrahydro-1H-indol-4-ylidene]amino acetate

There total 4 articles about [3-[(4-chlorophenyl)sulfanyl]-1-(2-ethoxy-2-oxoethyl)-2-methyl-4,5,6,7-tetrahydro-1H-indol-4-ylidene]amino acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1260673-30-0
ethyl [3-(4-chlorophenylsulfanyl)-4-(hydroxyimino)-2-methyl-4,5,6,7-tetrahydro-1H-indol-1-yl]acetate

: 108-24-7
acetic anhydride

: 1260673-32-2
[3-[(4-chlorophenyl)sulfanyl]-1-(2-ethoxy-2-oxoethyl)-2-methyl-4,5,6,7-tetrahydro-1H-indol-4-ylidene]amino acetate

Guidance literature:: With acetic acid; In xylene; at 20 ℃; for 0.333333h; Inert atmosphere;

Reference yield:

: 504-02-9
1,3-cylohexanedione

: 1260673-32-2
[3-[(4-chlorophenyl)sulfanyl]-1-(2-ethoxy-2-oxoethyl)-2-methyl-4,5,6,7-tetrahydro-1H-indol-4-ylidene]amino acetate

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium hydroxide / ethanol; water / 0.5 h / 20 - 30 °C / Inert atmosphere

1.2: 19 h / 20 °C / Inert atmosphere

2.1: sodium acetate / ethanol; water / 2 h / Reflux; Inert atmosphere; Industry scale

3.1: sulfuryl dichloride / ethyl acetate / 1 h / 0 °C / Inert atmosphere

3.2: 0.5 h / Inert atmosphere

3.3: 20 - 60 °C / Inert atmosphere

4.1: acetic acid / xylene / 0.33 h / 20 °C / Inert atmosphere

With sulfuryl dichloride; sodium acetate; acetic acid; potassium hydroxide; In ethanol; water; ethyl acetate; xylene;

Reference yield:

: 90534-62-6
2-(2-oxopropyl)cyclohexane-1,3-dione

: 1260673-32-2
[3-[(4-chlorophenyl)sulfanyl]-1-(2-ethoxy-2-oxoethyl)-2-methyl-4,5,6,7-tetrahydro-1H-indol-4-ylidene]amino acetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium acetate / ethanol; water / 2 h / Reflux; Inert atmosphere; Industry scale

2.1: sulfuryl dichloride / ethyl acetate / 1 h / 0 °C / Inert atmosphere

2.2: 0.5 h / Inert atmosphere

2.3: 20 - 60 °C / Inert atmosphere

3.1: acetic acid / xylene / 0.33 h / 20 °C / Inert atmosphere

With sulfuryl dichloride; sodium acetate; acetic acid; In ethanol; water; ethyl acetate; xylene;