(2-R,3-S,5-S)-1-O,3-O-di(p-chlorobenzoyl)-1,2,3,5,14,15-hexahydroxy-2,5-anhydropentadecane

Base Information

Chemical Name:(2-R,3-S,5-S)-1-O,3-O-di(p-chlorobenzoyl)-1,2,3,5,14,15-hexahydroxy-2,5-anhydropentadecane
CAS No.:206121-83-7
Molecular Formula:C₂₉H₃₆Cl₂O₇
Molecular Weight:567.507
Hs Code.:

Synonyms:(2-R,3-S,5-S)-1-O,3-O-di(p-chlorobenzoyl)-1,2,3,5,14,15-hexahydroxy-2,5-anhydropentadecane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2-R,3-S,5-S)-1-O,3-O-di(p-chlorobenzoyl)-1,2,3,5,14,15-hexahydroxy-2,5-anhydropentadecane

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Technology Process of (2-R,3-S,5-S)-1-O,3-O-di(p-chlorobenzoyl)-1,2,3,5,14,15-hexahydroxy-2,5-anhydropentadecane

There total 1 articles about (2-R,3-S,5-S)-1-O,3-O-di(p-chlorobenzoyl)-1,2,3,5,14,15-hexahydroxy-2,5-anhydropentadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 163364-37-2
(2-R,3-S,5-S)-1-O,3-O-di(p-chlorobenzoyl)-1,2,3,5-tetrahydroxy-2,5-anhydropentadec-14-ene

: 206121-83-7
(2-R,3-S,5-S)-1-O,3-O-di(p-chlorobenzoyl)-1,2,3,5,14,15-hexahydroxy-2,5-anhydropentadecane

Guidance literature:: With osmium(VIII) oxide; 4-methylmorpholine N-oxide; In water; acetone; tert-butyl alcohol; for 6h;
DOI:10.1080/07328319808004669

Reference yield: 90.0%

: 18162-48-6
tert-butyldimethylsilyl chloride

: 206121-83-7
(2-R,3-S,5-S)-1-O,3-O-di(p-chlorobenzoyl)-1,2,3,5,14,15-hexahydroxy-2,5-anhydropentadecane

: 206121-85-9
(2-R,3-S,5-S)-1-O,3-O-di(p-chlorobenzoyl)-14-O-15-O-di(t-butyldimethylsilyl)-1,2,3,5,14,15-hexahydroxy-2,5-anhydropentadecane

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; for 48h;
DOI:10.1080/07328319808004669

Reference yield:

: 206121-83-7
(2-R,3-S,5-S)-1-O,3-O-di(p-chlorobenzoyl)-1,2,3,5,14,15-hexahydroxy-2,5-anhydropentadecane

: 206121-87-1
(2R,3S,5S)-5-[9,10-Bis-(tert-butyl-dimethyl-silanyloxy)-decyl]-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-tetrahydro-furan-3-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / imidazole / dimethylformamide / 48 h

2: 90 percent / trimethylamine / tetrahydrofuran; H₂O / 3 h / 0 °C

3: 75 percent / pyridine

With pyridine; 1H-imidazole; trimethylamine; In tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1080/07328319808004669