pent-4-enyl 2-O-benzoyl-3-O-benzyl-5-O-(triisopropylsilyl)-α-D-arabinofuranoside

Base Information

Chemical Name:pent-4-enyl 2-O-benzoyl-3-O-benzyl-5-O-(triisopropylsilyl)-α-D-arabinofuranoside
CAS No.:915150-36-6
Molecular Formula:C₃₃H₄₈O₆Si
Molecular Weight:568.826
Hs Code.:

Synonyms:pent-4-enyl 2-O-benzoyl-3-O-benzyl-5-O-(triisopropylsilyl)-α-D-arabinofuranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of pent-4-enyl 2-O-benzoyl-3-O-benzyl-5-O-(triisopropylsilyl)-α-D-arabinofuranoside

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Technology Process of pent-4-enyl 2-O-benzoyl-3-O-benzyl-5-O-(triisopropylsilyl)-α-D-arabinofuranoside

There total 1 articles about pent-4-enyl 2-O-benzoyl-3-O-benzyl-5-O-(triisopropylsilyl)-α-D-arabinofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1-O-(2-O-benzoyl-3-O-benzyl-5-O-(triisopropylsilyl)-D-arabinofuranosyl) trichloroacetimidate

: 821-09-0
n-Pent-4-enyl alcohol

: 915150-36-6
pent-4-enyl 2-O-benzoyl-3-O-benzyl-5-O-(triisopropylsilyl)-α-D-arabinofuranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -40 - -30 ℃; for 0.666667h;
DOI:10.1021/jo061233x

Reference yield: 96.0%

: 915150-36-6
pent-4-enyl 2-O-benzoyl-3-O-benzyl-5-O-(triisopropylsilyl)-α-D-arabinofuranoside

: 765274-09-7
pent-4-enyl 2-O-benzoyl-3-O-benzyl-α-D-arabinofuranoside

Guidance literature:: With acetyl chloride; In methanol; dichloromethane; at 0 ℃; for 3h;
DOI:10.1021/jo061233x

Reference yield:

: 915150-36-6
pent-4-enyl 2-O-benzoyl-3-O-benzyl-5-O-(triisopropylsilyl)-α-D-arabinofuranoside

: 915150-24-2
pent-4-enyl 5-O-[2-O-benzoyl-3-O-benzyl-5-O-(triisopropylsilyl)-α-D-arabinofuranosyl]-2-O-benzoyl-3-O-benzyl-α-D-arabinofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / acetyl chloride / CH₂Cl₂; methanol / 3 h / 0 °C

2: 94 percent / TMSOTf / CH₂Cl₂ / 1 h / -40 - -30 °C

With trimethylsilyl trifluoromethanesulfonate; acetyl chloride; In methanol; dichloromethane;
DOI:10.1021/jo061233x