C₂₉H₃₁NO₆

Base Information

Chemical Name:C₂₉H₃₁NO₆
CAS No.:1645305-47-0
Molecular Formula:C₂₉H₃₁NO₆
Molecular Weight:489.568
Hs Code.:

C<sub>29</sub>H<sub>31</sub>NO<sub>6</sub>

Synonyms:C₂₉H₃₁NO₆

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₉H₃₁NO₆

Chemical Property:

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Technology Process of C₂₉H₃₁NO₆

There total 8 articles about C₂₉H₃₁NO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1629189-51-0
3-[(R,2E,4E)-6-(hydroxymethyl)-4-methylocta-2,4-dienoyl]-4-methoxy-5-[4-(4-methoxybenzyloxy)phenyl]pyridin-2(1H)-one

: 1645305-47-0
C₂₉H₃₁NO₆

Guidance literature:: With lithium iodide trihydrate; pyridine hydrochloride; In tetrahydrofuran; at 60 ℃; for 4h; Microwave irradiation;
DOI:10.1055/s-0033-1340868

Reference yield:

: 1321530-50-0
(E)-methyl 2-(((tert-butyldimethylsilyl)oxy)methyl)but-2-enoate

: 1645305-47-0
C₂₉H₃₁NO₆

Guidance literature:: Multi-step reaction with 8 steps

1: C₂₆H₂₂NOP*C₃₂H₁₂BF₂₄^(1-)*C₈H₁₂*Ir⁽¹⁺⁾; hydrogen / dichloromethane / 16 h / 20 °C / 37503.8 Torr / Autoclave

2: diisobutylaluminium hydride / dichloromethane / 1 h / -78 °C

3: dichloromethane / 48 h / Reflux

4: diisobutylaluminium hydride / tetrahydrofuran; hexane / 1.83 h / -78 - 20 °C

5: 4-methylmorpholine N-oxide; tetrapropylammonium perruthennate / dichloromethane / 1 h / 20 °C / Molecular sieve

6: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

7: lithium hydroxide monohydrate / water; tetrahydrofuran / 144 h / 20 °C / Darkness

8: lithium iodide trihydrate; pyridine hydrochloride / tetrahydrofuran / 4 h / 60 °C / Microwave irradiation

With tetrapropylammonium perruthennate; lithium iodide trihydrate; lithium hydroxide monohydrate; C₂₆H₂₂NOP*C₃₂H₁₂BF₂₄^(1-)*C₈H₁₂*Ir⁽¹⁺⁾; tetrabutyl ammonium fluoride; hydrogen; pyridine hydrochloride; diisobutylaluminium hydride; 4-methylmorpholine N-oxide; In tetrahydrofuran; hexane; dichloromethane; water;
DOI:10.1055/s-0033-1340868

Reference yield:

: 339533-79-8
(2S)-2-ethyl-3-[(tert-butyldiphenylsilyl)oxy]propanal

: 1645305-47-0
C₂₉H₃₁NO₆

Guidance literature:: Multi-step reaction with 6 steps

1: dichloromethane / 48 h / Reflux

2: diisobutylaluminium hydride / tetrahydrofuran; hexane / 1.83 h / -78 - 20 °C

3: 4-methylmorpholine N-oxide; tetrapropylammonium perruthennate / dichloromethane / 1 h / 20 °C / Molecular sieve

4: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

5: lithium hydroxide monohydrate / water; tetrahydrofuran / 144 h / 20 °C / Darkness

6: lithium iodide trihydrate; pyridine hydrochloride / tetrahydrofuran / 4 h / 60 °C / Microwave irradiation

With tetrapropylammonium perruthennate; lithium iodide trihydrate; lithium hydroxide monohydrate; tetrabutyl ammonium fluoride; pyridine hydrochloride; diisobutylaluminium hydride; 4-methylmorpholine N-oxide; In tetrahydrofuran; hexane; dichloromethane; water;
DOI:10.1055/s-0033-1340868