4-((2-chlorophenyl)(3,4-dimethoxyphenyl)methyl)-1,2-dimethoxybenzene

Base Information

• Chemical Name: 4-((2-chlorophenyl)(3,4-dimethoxyphenyl)methyl)-1,2-dimethoxybenzene
• CAS No.: 1280728-62-2
• Molecular Formula: C₂₃H₂₃ClO₄
• Molecular Weight: 398.886
• Mol file: 1280728-62-2.mol

Synonyms:4-((2-chlorophenyl)(3,4-dimethoxyphenyl)methyl)-1,2-dimethoxybenzene

Chemical Property of 4-((2-chlorophenyl)(3,4-dimethoxyphenyl)methyl)-1,2-dimethoxybenzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-((2-chlorophenyl)(3,4-dimethoxyphenyl)methyl)-1,2-dimethoxybenzene

There total 1 articles about 4-((2-chlorophenyl)(3,4-dimethoxyphenyl)methyl)-1,2-dimethoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

1,2-dimethoxybenzene (91-16-7) + 2-chloro-benzaldehyde (89-98-5) → 4-((2-chlorophenyl)(3,4-dimethoxyphenyl)methyl)-1,2-dimethoxybenzene (1280728-62-2)

Guidance literature:

With silica sulfuric acid; at 65 ℃; for 0.333333h; Neat (no solvent);

DOI:10.1016/j.crci.2011.02.009

Reference yield:

4-((2-chlorophenyl)(3,4-dimethoxyphenyl)methyl)-1,2-dimethoxybenzene (1280728-62-2) + 1,1-diacetoxy-1-(2-chlorophenyl)methane (13086-95-8) → 9,10-bis(2-chlorophenyl)-2,3,6,7-tetramethoxyanthracene (1280728-80-4)

Guidance literature:

With phosphotungstic acid; acetic acid; at 60 ℃; for 1h;

DOI:10.1002/ejoc.201001267

Reference yield:

4-((2-chlorophenyl)(3,4-dimethoxyphenyl)methyl)-1,2-dimethoxybenzene (1280728-62-2) + 2-chloro-benzaldehyde (89-98-5) → 9,10-bis(2-chlorophenyl)-2,3,6,7-tetramethoxyanthracene (1280728-80-4)

Guidance literature:

With phosphotungstic acid; acetic anhydride; acetic acid; at 75 ℃; for 1.5h;

DOI:10.1002/ejoc.201001267

upstream raw materials:

1,2-dimethoxybenzene

2-chloro-benzaldehyde

Downstream raw materials:

9,10-bis(2-chlorophenyl)-2,3,6,7-tetramethoxyanthracene

10-(3-bromophenyl)-9-(2-chlorophenyl)-2,3,6,7-tetramethoxyanthracene