2,6-diacetylpyridine bis(⁴N-4-(p-chlorophenyl)-3-thiosemicarbazonato)palladium(II)

Base Information

• Chemical Name: 2,6-diacetylpyridine bis(⁴N-4-(p-chlorophenyl)-3-thiosemicarbazonato)palladium(II)
• CAS No.: 1620144-07-1
• Molecular Formula: C₂₃H₁₉Cl₂N₇PdS₂
• Molecular Weight: 634.909

Synonyms:2,6-diacetylpyridine bis(⁴N-4-(p-chlorophenyl)-3-thiosemicarbazonato)palladium(II)

Chemical Property of 2,6-diacetylpyridine bis(⁴N-4-(p-chlorophenyl)-3-thiosemicarbazonato)palladium(II)

Chemical Property:

Purity/Quality:

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Technology Process of 2,6-diacetylpyridine bis(⁴N-4-(p-chlorophenyl)-3-thiosemicarbazonato)palladium(II)

There total 3 articles about 2,6-diacetylpyridine bis(⁴N-4-(p-chlorophenyl)-3-thiosemicarbazonato)palladium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

bis-triphenylphosphine-palladium(II) chloride (13965-03-2) + 2,6-diacetylpyridine bis(4N-p-chlorophenylthiosemicarbazone) (201360-06-7) → 2,6-diacetylpyridine bis(4N-4-(p-chlorophenyl)-3-thiosemicarbazonato)palladium(II) (1620144-07-1)

Guidance literature:

With triethylamine; In toluene; at 20 ℃; for 20h;

DOI:10.1016/j.jinorgbio.2014.04.017

Reference yield:

4-Chlorophenyl isothiocyanate (2131-55-7) → 2,6-diacetylpyridine bis(4N-4-(p-chlorophenyl)-3-thiosemicarbazonato)palladium(II) (1620144-07-1)

Guidance literature:

Multi-step reaction with 3 steps

1: hydrazine hydrate / ethanol / 1 h

2: ethanol / 5 h

3: triethylamine / toluene / 20 h / 20 °C

With hydrazine hydrate; triethylamine; In ethanol; toluene;

DOI:10.1016/j.jinorgbio.2014.04.017

Reference yield:

4-(p-chlorophenyl)-3-thiosemicarbazide (22814-92-2) → 2,6-diacetylpyridine bis(4N-4-(p-chlorophenyl)-3-thiosemicarbazonato)palladium(II) (1620144-07-1)

Guidance literature:

Multi-step reaction with 2 steps

1: ethanol / 5 h

2: triethylamine / toluene / 20 h / 20 °C

With triethylamine; In ethanol; toluene;

DOI:10.1016/j.jinorgbio.2014.04.017

upstream raw materials:

bis-triphenylphosphine-palladium(II) chloride

2,6-diacetylpyridine bis(⁴N-p-chlorophenylthiosemicarbazone)

4-Chlorophenyl isothiocyanate

4-(p-chlorophenyl)-3-thiosemicarbazide

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